{3-[(E)-2-pyridin-4-ylvinyl]phenyl}amine

Base Information

Chemical Name:{3-[(E)-2-pyridin-4-ylvinyl]phenyl}amine
CAS No.:32598-04-2
Molecular Formula:C13H12N2
Molecular Weight:196.252
Hs Code.:
NSC Number:204928
DSSTox Substance ID:DTXSID60357229
Wikidata:Q82137049
Pharos Ligand ID:8YQ5XH7VZJ8K
ChEMBL ID:CHEMBL3193752

Synonyms:1401774-23-9;{3-[(E)-2-pyridin-4-ylvinyl]phenyl}amine;3-[(E)-2-pyridin-4-ylethenyl]aniline;MLS000756475;(E)-3-(2-(Pyridin-4-yl)vinyl)aniline;3-[(1E)-2-(pyridin-4-yl)ethenyl]aniline;32598-04-2;(3-[(E)-2-Pyridin-4-ylvinyl]phenyl)amine;NSC204928;4-(m-aminostyryl-)pyridin;CHEMBL3193752;SCHEMBL12760703;SCHEMBL12760704;DTXSID60357229;HMS1605L17;HMS2886J21;MFCD03942178;STK228669;AKOS003297221;NSC-204928;(E)-3-(2-pyridin-4-ylvinyl)phenylamine;LS-08745;SMR000528751;3-[(E)-2-(pyridin-4-yl)ethenyl]aniline;Benzenamine, 3-[2-(4-pyridinyl)ethenyl]-

Suppliers and Price of {3-[(E)-2-pyridin-4-ylvinyl]phenyl}amine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of {3-[(E)-2-pyridin-4-ylvinyl]phenyl}amine

Chemical Property:

Vapor Pressure:3E-06mmHg at 25°C
Boiling Point:388.7°C at 760 mmHg
Flash Point:217.3°C
Density:1.167g/cm³
XLogP3:2.4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:196.100048391
Heavy Atom Count:15
Complexity:207

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=CC(=C1)N)C=CC2=CC=NC=C2
Isomeric SMILES:C1=CC(=CC(=C1)N)/C=C/C2=CC=NC=C2

Technology Process of {3-[(E)-2-pyridin-4-ylvinyl]phenyl}amine

There total 5 articles about {3-[(E)-2-pyridin-4-ylvinyl]phenyl}amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 46837-95-0,76024-00-5
4-[2-(3-nitrophenyl)ethenyl]pyridine

: 32598-04-2
(E)-3-(2-(pyridin-4-yl)vinyl)aniline

Guidance literature:: 4-[2-(3-nitrophenyl)ethenyl]pyridine; With tin(II) chloride dihdyrate; ethanol; at 60 ℃; for 16h; Inert atmosphere;

With sodium hydroxide; In water; ethyl acetate; Product distribution / selectivity;

Reference yield: 72.0%

: 100-43-6,329041-72-7
4-vinylpyridine

: 591-19-5
m-Bromoaniline

: 32598-04-2
(E)-3-(2-(pyridin-4-yl)vinyl)aniline

Guidance literature:: With piperidine; diamminedichloropalladium(II); In N,N-dimethyl-formamide; at 140 ℃; for 1.5h; Inert atmosphere; Sealed tube; Microwave irradiation;
DOI:10.1039/c5md00197h

Reference yield:

: 100-43-6,329041-72-7
4-vinylpyridine

: 32598-04-2
(E)-3-(2-(pyridin-4-yl)vinyl)aniline

Guidance literature:: Multi-step reaction with 2 steps

1: sodium acetate / triphenylphosphine; palladium diacetate / N,N-dimethyl-formamide / 24 h / 135 °C / Inert atmosphere

2: ethanol; tin(II) chloride dihdyrate / 16 h / 60 °C / Inert atmosphere

With tin(II) chloride dihdyrate; ethanol; sodium acetate; palladium diacetate; triphenylphosphine; In N,N-dimethyl-formamide;