Hexamethyldigermoxane

Base Information

Chemical Name:Hexamethyldigermoxane
CAS No.:2237-93-6
Molecular Formula:C₆H₁₈Ge₂O
Molecular Weight:251.388
Hs Code.:
DSSTox Substance ID:DTXSID70586664
Nikkaji Number:J151.308G
NSC Number:92303
Wikidata:Q82478818
Mol file:2237-93-6.mol

Synonyms:2237-93-6;Hexamethyldigermoxane;hexamethyldigermoxan;SCHEMBL7716224;DTXSID70586664;NSC92303;NSC-92303

Suppliers and Price of Hexamethyldigermoxane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of Hexamethyldigermoxane

Chemical Property:

Boiling Point:°Cat760mmHg
Flash Point:°C
PSA：9.23000
Density:g/cm³
LogP:2.67280
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:251.9790188
Heavy Atom Count:9
Complexity:76.2

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C[Ge](C)(C)O[Ge](C)(C)C

Technology Process of Hexamethyldigermoxane

There total 11 articles about Hexamethyldigermoxane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 59579-33-8
bis(trimethylgermyl)carbodiimide

: (H₂NCN)2

: 2237-93-6
hexamethyldigermoxane

Guidance literature:: With water; In neat (no solvent); condensation of excess of water onto Ge-compd. (-196°C), warming to room temp., standing for 60 min; fractional low-temp. distn. (collection of excess water at -23°C,of product at -196°C);
DOI:10.1039/DT9760000366

Reference yield: 79.0%

: 124-38-9,18923-20-1
carbon dioxide

: (η⁵-C₅Me₅)*Mo{N(iPr)C(Me)N(iPr)}(NGeMe₃)

: 1529-47-1
chlorotrimethylgermane

: (η⁵-C₅Me₅)*Mo{N(iPr)C(Me)N(iPr)}Cl₂

: 2237-93-6
hexamethyldigermoxane

: 7514-86-5
trimethylgermyl isocyanate

Guidance literature:: With 1,2,4,5-tetramethylbenzene; In benzene-d6; at 75 ℃; for 72h; under 1034.32 Torr; Sealed tube;
DOI:10.1002/anie.201502293

Reference yield: 23.0%

: 392245-45-3
2,6-diethyl-4,8-dimethyl-2,3,6,7 tetrahydro-s-indacene-1,5-dione

: 13361-67-6
(dimethylamino)trimethylgermane

: 697745-59-8
((CH₃)2N)(OGe(CH₃)3)C₁₂H₆(C₂H₅)2(CH₃)2(O)

: 2237-93-6
hexamethyldigermoxane

Guidance literature:: In not given; mixt. of Ge comp. and diketone was kept for 6 h at 20°C, then heated in Carius tube at 100°C for 6 h; mixt. was analyzed by GC, GC/Mas;
DOI:10.1016/j.ica.2003.10.017