(4E)-4-({[4-(2-chloro-10,11-dihydrodibenzo[b,f]thiepin-10-yl)piperazin-1-yl]amino}methylidene)-2-ethoxycyclohexa-2,5-dien-1-one

Base Information

Chemical Name:(4E)-4-({[4-(2-chloro-10,11-dihydrodibenzo[b,f]thiepin-10-yl)piperazin-1-yl]amino}methylidene)-2-ethoxycyclohexa-2,5-dien-1-one
CAS No.:86759-01-5
Molecular Formula:C₂₇H₂₈ClN₃O₂S
Molecular Weight:494.057
Hs Code.:

Synonyms:Dibenzo[b,f]thiepin,phenol deriv.

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (4E)-4-({[4-(2-chloro-10,11-dihydrodibenzo[b,f]thiepin-10-yl)piperazin-1-yl]amino}methylidene)-2-ethoxycyclohexa-2,5-dien-1-one

Chemical Property:

Vapor Pressure:3.49E-15mmHg at 25°C
Boiling Point:617.6°Cat760mmHg
Flash Point:327.3°C
Density:1.35g/cm³

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (4E)-4-({[4-(2-chloro-10,11-dihydrodibenzo[b,f]thiepin-10-yl)piperazin-1-yl]amino}methylidene)-2-ethoxycyclohexa-2,5-dien-1-one

There total 3 articles about (4E)-4-({[4-(2-chloro-10,11-dihydrodibenzo[b,f]thiepin-10-yl)piperazin-1-yl]amino}methylidene)-2-ethoxycyclohexa-2,5-dien-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 86759-17-3
2-chloro-10-(4-nitrosopiperazino)-10,11-dihydrodibenzothiepin

: 86759-01-5
2-chloro-10-<4-(3-ethoxy-4-hydroxybenzylideneamino)piperazino>-10,11-dihydrodibenzothiepin

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / LiAlH₄ / diethyl ether / 5 h / Ambient temperature

2: ethanol / 1 h / Heating

With lithium aluminium tetrahydride; In diethyl ether; ethanol;
DOI:10.1135/cccc19831173

Reference yield:

: 52548-24-0
1-(2-chloro-10,11-dihydro-dibenzo[b,f]thiepin-10-yl)-piperazine

: 86759-01-5
2-chloro-10-<4-(3-ethoxy-4-hydroxybenzylideneamino)piperazino>-10,11-dihydrodibenzothiepin

Guidance literature:: Multi-step reaction with 3 steps

1: 76 percent / NaNO₂, aq. HCl / 1.) 75-80 deg C, 3 h, 2.) R_.T_., overnight.

2: 97 percent / LiAlH₄ / diethyl ether / 5 h / Ambient temperature

3: ethanol / 1 h / Heating

With hydrogenchloride; lithium aluminium tetrahydride; sodium nitrite; In diethyl ether; ethanol;
DOI:10.1135/cccc19831173