diethyl [4-(2-ethoxy-2-oxoethyl)-3-phenyl-1,3-thiazol-2(3H)-ylidene]propanedioate

Base Information

Chemical Name:diethyl [4-(2-ethoxy-2-oxoethyl)-3-phenyl-1,3-thiazol-2(3H)-ylidene]propanedioate
CAS No.:84645-54-5
Molecular Formula:C20H23 N O6 S
Molecular Weight:405.4647
Hs Code.:

Synonyms:Propanedioicacid, [4-(2-ethoxy-2-oxoethyl)-3-phenyl-2(3H)-thiazolylidene]-, diethyl ester(9CI); NSC 373928

Suppliers and Price of diethyl [4-(2-ethoxy-2-oxoethyl)-3-phenyl-1,3-thiazol-2(3H)-ylidene]propanedioate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 2 raw suppliers

Chemical Property of diethyl [4-(2-ethoxy-2-oxoethyl)-3-phenyl-1,3-thiazol-2(3H)-ylidene]propanedioate

Chemical Property:

Vapor Pressure:9.81E-09mmHg at 25°C
Boiling Point:462.5°Cat760mmHg
Flash Point:233.5°C
Density:1.252g/cm³

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of diethyl [4-(2-ethoxy-2-oxoethyl)-3-phenyl-1,3-thiazol-2(3H)-ylidene]propanedioate

There total 8 articles about diethyl [4-(2-ethoxy-2-oxoethyl)-3-phenyl-1,3-thiazol-2(3H)-ylidene]propanedioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 84645-57-8
ethyl 2-diethoxycarbonylmethylene-4-hydroxy-3-phenylthiazolidine-4-acetate

: 84645-54-5
ethyl 2-diethoxycarbonylmethylene-3-phenyl-4-thiazoline-4-acetate

Guidance literature:: With toluene-4-sulfonic acid; In benzene; for 2h; Heating;

Reference yield:

: 638-07-3
ethyl (2-chloroaceto)acetate

: 84645-54-5
ethyl 2-diethoxycarbonylmethylene-3-phenyl-4-thiazoline-4-acetate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) sodium ethoxide / 1.) ethanol room temp., 1.5 h, 2.) ethanol, room temp., 1.5 h

2: 84 percent / p-toluenesulfonic acid / benzene / 2 h / Heating

With sodium ethanolate; toluene-4-sulfonic acid; In benzene;

Reference yield:

: 13176-46-0
4-bromoethyl acetoacetate

: 84645-54-5
ethyl 2-diethoxycarbonylmethylene-3-phenyl-4-thiazoline-4-acetate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) sodium ethoxide / 1.) ethanol room temp., 1.5 h, 2.) ethanol, room temp., 1.5 h

2: 84 percent / p-toluenesulfonic acid / benzene / 2 h / Heating

With sodium ethanolate; toluene-4-sulfonic acid; In benzene;