Benzaldehyde, p-(dimethylamino)-, (p-bromophenyl)hydrazone

Base Information

• Chemical Name: Benzaldehyde, p-(dimethylamino)-, (p-bromophenyl)hydrazone
• CAS No.: 27246-80-6
• Molecular Formula: C15H16 Br N3
• Molecular Weight: 318.2116
• Mol file: 27246-80-6.mol

Synonyms:BRN 3350109;(p-Dimethylamino)benzaldehyde p-bromophenylhydrazone;Benzaldehyde, p-(dimethylamino)-, (p-bromophenyl)hydrazone;0-15-00-00449 (Beilstein Handbook Reference);27246-80-6;C15H16BrN3;C15-H16-Br-N3;LS-25026

Chemical Property of Benzaldehyde, p-(dimethylamino)-, (p-bromophenyl)hydrazone

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• Boiling Point: 427.494°C at 760 mmHg
• Flash Point: 212.341°C
• Density: 1.282g/cm³
• XLogP3: 4.4
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 4
• Exact Mass: 317.05276
• Heavy Atom Count: 19
• Complexity: 277

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CN(C)C1=CC=C(C=C1)C=NNC2=CC=C(C=C2)Br
• Isomeric SMILES: CN(C)C1=CC=C(C=C1)/C=N/NC2=CC=C(C=C2)Br

Technology Process of Benzaldehyde, p-(dimethylamino)-, (p-bromophenyl)hydrazone

There total 1 articles about Benzaldehyde, p-(dimethylamino)-, (p-bromophenyl)hydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-dimethylamino-benzaldehyde (100-10-7) + (4-bromophenyl)hydrazine (589-21-9) → 4-dimethylamino-benzaldehyde-(4-bromo-phenylhydrazone) (27246-80-6)

Guidance literature:

Reference yield: 55.0%

pyridine (110-86-1) + 4-dimethylamino-benzaldehyde-(4-bromo-phenylhydrazone) (27246-80-6) → 1-(4-Bromo-phenyl)-3-(4-dimethylamino-phenyl)-1H-[1,2,4]triazolo[4,3-a]pyridin-4-ylium; perchlorate (115095-10-8)

Guidance literature:

With tetraethylammonium perchlorate; In acetonitrile; electrochemical oxidation;

DOI:10.1021/jo00256a033

upstream raw materials:

4-dimethylamino-benzaldehyde

(4-bromophenyl)hydrazine

Downstream raw materials:

1-(4-Bromo-phenyl)-3-(4-dimethylamino-phenyl)-1H-[1,2,4]triazolo[4,3-a]pyridin-4-ylium; perchlorate