p-(2,2-Dimethoxyethoxy)anisole

Base Information

Chemical Name:p-(2,2-Dimethoxyethoxy)anisole
CAS No.:68426-08-4
Deprecated CAS:93882-06-5
Molecular Formula:C11H16O4
Molecular Weight:212.246
Hs Code.:
European Community (EC) Number:270-388-6
UNII:TPM24DL6HV
DSSTox Substance ID:DTXSID1071535
Nikkaji Number:J332.551B
Wikidata:Q81999208
Mol file:68426-08-4.mol

Synonyms:p-(2,2-Dimethoxyethoxy)anisole;1-(2,2-dimethoxyethoxy)-4-methoxybenzene;68426-08-4;p-Methoxyphenoxyacetaldehyde dimethylacetal;Benzene, 1-(2,2-dimethoxyethoxy)-4-methoxy-;EINECS 270-388-6;4-methoxy-(2,2-dimethoxy)ethoxybenzene;TPM24DL6HV;C9H21O3PS;SCHEMBL7931690;DTXSID1071535;C9-H21-O3-P-S;Ethyl pentyl phosphorothioate (7CI);AKOS015567657;p-methoxy phenoxy acetaldehyde dimethyl acetal

Suppliers and Price of p-(2,2-Dimethoxyethoxy)anisole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Atlantic Research Chemicals
1-(2,2-Dimethoxyethoxy)-4-methoxybenzene 95%
10gm:
$ 600.88

Atlantic Research Chemicals
1-(2,2-Dimethoxyethoxy)-4-methoxybenzene 95%
1gm:
$ 74.23

Total 7 raw suppliers

Chemical Property of p-(2,2-Dimethoxyethoxy)anisole

Chemical Property:

Vapor Pressure:0.00228mmHg at 25°C
Refractive Index:1.481
Boiling Point:298.2°C at 760 mmHg
Flash Point:113.8°C
PSA：36.92000
Density:1.06g/cm³
LogP:1.69290
XLogP3:1.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:6
Exact Mass:212.10485899
Heavy Atom Count:15
Complexity:151

Purity/Quality:

99% ^*data from raw suppliers

1-(2,2-Dimethoxyethoxy)-4-methoxybenzene 95% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC=C(C=C1)OCC(OC)OC

Technology Process of p-(2,2-Dimethoxyethoxy)anisole

There total 2 articles about p-(2,2-Dimethoxyethoxy)anisole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 7252-83-7
1-bromo-2,2-dimethoxyethane

: 150-76-5
4-methoxy-phenol

: 68426-08-4
1-(2,2-dimethoxyethoxy)-4-methoxybenzene

Guidance literature:: 4-methoxy-phenol; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 - 20 ℃;

1-bromo-2,2-dimethoxyethane; In N,N-dimethyl-formamide; mineral oil; at 120 ℃;
DOI:10.1002/chem.201804515

Reference yield:

: 97-97-2
chloroacetaldehyde dimethyl acetal

: 150-76-5
4-methoxy-phenol

: 68426-08-4
1-(2,2-dimethoxyethoxy)-4-methoxybenzene

Guidance literature:: 4-methoxy-phenol; In N,N-dimethyl-formamide; at 60 ℃; Inert atmosphere;

chloroacetaldehyde dimethyl acetal; In N,N-dimethyl-formamide; at 150 ℃; Inert atmosphere;
DOI:10.1021/acs.orglett.0c01655

Reference yield:

: 68426-08-4
1-(2,2-dimethoxyethoxy)-4-methoxybenzene

: 4-((5-methoxy-1a,6b-dihydro-1H-cyclopropa[b]benzofuran-1-yl)methylene)-1-tosylpiperidine

Guidance literature:: Multi-step reaction with 2 steps

1: phosphoric acid / chlorobenzene / 130 °C / Inert atmosphere

2: dirhodium tetraacetate / dichloromethane / 21 h / 20 °C / Inert atmosphere; Sealed tube

With dirhodium tetraacetate; phosphoric acid; In dichloromethane; chlorobenzene;
DOI:10.1021/acs.orglett.0c01655