methyl N-[(4-methylphenyl)sulfonyl]phenylalaninate

Base Information

• Chemical Name: methyl N-[(4-methylphenyl)sulfonyl]phenylalaninate
• CAS No.: 42384-33-8
• Molecular Formula: C₁₇H₁₉NO₄S
• Molecular Weight: 333.408
• Mol file: 42384-33-8.mol

Synonyms:Methyl(2S)-2-[[(4-methylphenyl)sulfonyl]amino]-3-phenylpropanoate; Methyl2-(4-methylphenylsulfonamido)-3-phenylpropanoate; NSC 339917

Chemical Property of methyl N-[(4-methylphenyl)sulfonyl]phenylalaninate

Chemical Property:

• Vapor Pressure: 7.41E-10mmHg at 25°C
• Boiling Point: 492.8°Cat760mmHg
• Flash Point: 251.9°C
• Density: 1.233g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of methyl N-[(4-methylphenyl)sulfonyl]phenylalaninate

There total 22 articles about methyl N-[(4-methylphenyl)sulfonyl]phenylalaninate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

methyl (2S)-2-amino-3-phenylpropanoate (2577-90-4) + p-toluenesulfonyl chloride (98-59-9) → N-(p-toluenesulfonyl)-L-phenylalanine methyl ester (51220-86-1,149703-21-9,42384-33-8)

Guidance literature:

With triethylamine; In dichloromethane; at 20 ℃; for 12h; Inert atmosphere;

DOI:10.1039/c5cc01716e

Reference yield: 99.0%

C22H27NO6S → N-(p-toluenesulfonyl)-L-phenylalanine methyl ester (51220-86-1,149703-21-9,42384-33-8)

Guidance literature:

With iron(III) chloride; chloro-trimethyl-silane; In dichloromethane; at 20 ℃;

DOI:10.1039/c4ra12143k

Reference yield: 96.0%

methyl (2S)-2-amino-3-phenylpropanoate hydrochloride (7524-50-7) + p-toluenesulfonyl chloride (98-59-9) → N-(p-toluenesulfonyl)-L-phenylalanine methyl ester (51220-86-1,149703-21-9,42384-33-8)

Guidance literature:

With triethylamine; In dichloromethane; at 20 ℃; for 20h;

upstream raw materials:

cis-(2S,3S)-(+)-N-(p-toluenesulfonyl)-2-carbomethoxy-3-phenylaziridine

methyl (((9H-fluoren-9-yl)methoxy)carbonyl)-L-phenylalaninate

p-toluenesulfonyl chloride

ester methylique de la N-tosyl β-iodo L-alanine

Downstream raw materials:

N-(1-benzyl-2-hydroxy-2-vinyl-but-3-enyl)-4-methyl-benzenesulfonamide

(2S)-2-p-toluenesulfonamido-3-phenylpropanol

dimethyl (S)-3-[(p-toluenesulfonyl)amino]-2-oxo-4-phenylbutylphosphonate

(S)-N-(1-benzyl-2-hydroxyethyl)hexadecanamide

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