Propylamine, N-(2-chloroethyl)-N-methyl-3-(triethylsilyl)-, hydrochloride

Base Information

Chemical Name:Propylamine, N-(2-chloroethyl)-N-methyl-3-(triethylsilyl)-, hydrochloride
CAS No.:84584-74-7
Molecular Formula:C₁₂H₂₈ClNSi*ClH
Molecular Weight:286.36
Hs Code.:2931900090
DSSTox Substance ID:DTXSID30233566
Mol file:84584-74-7.mol

Synonyms:Propylamine, N-(2-chloroethyl)-N-methyl-3-(triethylsilyl)-, hydrochloride;84584-74-7;N-(2-Chloroethyl)-N-methyl-3-(triethylsilyl)propylamine hydrochloride;1-Propanamine, N-(2-chloroethyl)-N-methyl-3-(triethylsilyl)-, hydrochloride;C12H28ClNSi.ClH;C12-H28-Cl-N-Si.Cl-H;DTXSID30233566;LS-125569

Suppliers and Price of Propylamine, N-(2-chloroethyl)-N-methyl-3-(triethylsilyl)-, hydrochloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
1-PROPANAMINE, N-(2-CHLOROETHYL)-N-METHYL-3-(TRIETHYLSILYL)-, HYDROCHL ORIDE 95.00%
5MG
$ 496.24

Total 4 raw suppliers

Chemical Property of Propylamine, N-(2-chloroethyl)-N-methyl-3-(triethylsilyl)-, hydrochloride

Chemical Property:

Vapor Pressure:0.0136mmHg at 25°C
Boiling Point:258.6°C at 760 mmHg
Flash Point:110.2°C
PSA：3.24000
LogP:4.85760
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:9
Exact Mass:285.1446319
Heavy Atom Count:16
Complexity:140

Purity/Quality:

99% ^*data from raw suppliers

1-PROPANAMINE, N-(2-CHLOROETHYL)-N-METHYL-3-(TRIETHYLSILYL)-, HYDROCHL ORIDE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC[Si](CC)(CC)CCCN(C)CCCl.Cl

Technology Process of Propylamine, N-(2-chloroethyl)-N-methyl-3-(triethylsilyl)-, hydrochloride

There total 2 articles about Propylamine, N-(2-chloroethyl)-N-methyl-3-(triethylsilyl)-, hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 67039-16-1
2-amino>ethanol

: 84584-74-7
(2-Chloro-ethyl)-methyl-(3-triethylsilanyl-propyl)-amine; hydrochloride

Guidance literature:: With thionyl chloride; In chloroform; at 35 - 40 ℃; for 4h;
DOI:10.1007/BF00772158

Reference yield:

: 2290-35-9
(3-chloropropyl)triethylsilane

: 84584-74-7
(2-Chloro-ethyl)-methyl-(3-triethylsilanyl-propyl)-amine; hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 54 percent / Et₃N / butan-1-ol / 22 h / Heating

2: 70 percent / SOCl₂ / CHCl₃ / 4 h / 35 - 40 °C

With thionyl chloride; triethylamine; In chloroform; butan-1-ol;
DOI:10.1007/BF00772158

Reference yield:

: 84584-74-7
(2-Chloro-ethyl)-methyl-(3-triethylsilanyl-propyl)-amine; hydrochloride

: 74-88-4
methyl iodide

: 84584-77-0
(2-Chloro-ethyl)-dimethyl-(3-triethylsilanyl-propyl)-ammonium; iodide

Guidance literature:: With potassium hydroxide; Yield given. Multistep reaction; 1.) ether, 2.) ether, 35-40 deg C, 4 h; 20 deg C, 16 h;
DOI:10.1007/BF00772158