1,4-Dioxan-2-yl(phenyl)methanone

Base Information

Chemical Name:1,4-Dioxan-2-yl(phenyl)methanone
CAS No.:5397-44-4
Molecular Formula:C11H12O3
Molecular Weight:192.214
Hs Code.:
NSC Number:4208
DSSTox Substance ID:DTXSID001305716

Synonyms:5397-44-4;NSC4208;1,4-Dioxan-2-ylphenylmethanone;DTXSID001305716;NSC-4208;AKOS012094331

Suppliers and Price of 1,4-Dioxan-2-yl(phenyl)methanone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 1,4-Dioxan-2-yl(phenyl)methanone

Chemical Property:

Vapor Pressure:0.000382mmHg at 25°C
Boiling Point:317.6°C at 760 mmHg
Flash Point:136.9°C
Density:1.161g/cm³
XLogP3:1.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:192.078644241
Heavy Atom Count:14
Complexity:197

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1COC(CO1)C(=O)C2=CC=CC=C2

Technology Process of 1,4-Dioxan-2-yl(phenyl)methanone

There total 3 articles about 1,4-Dioxan-2-yl(phenyl)methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 123-91-1,28347-88-8,28347-91-3,39449-24-6,54841-74-6
1,4-dioxane

: 6343-27-7
1-benzoylpyrrolidine-2,5-dione

: 5397-44-4
(1,4-dioxan-2-yl)(phenyl)methanone

Guidance literature:: With potassium phosphate; [4,4′-bis(1,1-dimethylethyl)-2,2′-bipyridine-N1,N1′]bis{3,5-difluoro-2-[5-(trifluoromethyl)-2-pyridinyl-κN]phenyl-κC}iridium(III) hexafluorophosphate; tetraaqua[4,4′-bis(1,1-dimethylethyl)-2,2′-bipyridine-N1,N1′]nickel(II) chloride; lithium chloride; at 20 ℃; for 24h; Reagent/catalyst; Inert atmosphere; Sealed tube; Irradiation;
DOI:10.1055/s-0040-1707301

Reference yield: 45.0%

: 123-91-1,28347-88-8,28347-91-3,39449-24-6,54841-74-6
1,4-dioxane

: 98-88-4
benzoyl chloride

: 5397-44-4
(1,4-dioxan-2-yl)(phenyl)methanone

Guidance literature:: With potassium phosphate; [4,4′-bis(1,1-dimethylethyl)-2,2′-bipyridine-N1,N1′]bis{3,5-difluoro-2-[5-(trifluoromethyl)-2-pyridinyl-κN]phenyl-κC}iridium(III) hexafluorophosphate; C₁₈H₂₄N₂*NiCl₂; at 20 ℃; for 24h; Inert atmosphere; Sealed tube; Irradiation;
DOI:10.1021/acs.orglett.7b01552

Reference yield:

: 5397-44-4
(1,4-dioxan-2-yl)(phenyl)methanone

Guidance literature:: With diethyl ether; phenylmagnesium bromide; Behandeln der Reaktionsloesung mit wss. Salzsaeure;
DOI:10.1021/ja01611a096