DIETHYL 3-METHYLCYCLOHEX-1-ENYLPHOSPHONATE

Base Information

• Chemical Name: DIETHYL 3-METHYLCYCLOHEX-1-ENYLPHOSPHONATE
• CAS No.: 126424-00-8
• Molecular Formula: C₁₁H₂₁O₄P
• Molecular Weight: 248.259
• Mol file: 126424-00-8.mol

Synonyms:Phosphoric acid,diethyl 3-methyl-1-cyclohexen-1-yl ester;

Chemical Property of DIETHYL 3-METHYLCYCLOHEX-1-ENYLPHOSPHONATE

Chemical Property:

• Vapor Pressure: 0.00431mmHg at 25°C
• Refractive Index: 1.449-1.451
• Boiling Point: 96 °C (4 mmHg)
• Flash Point: 141.5°C
• PSA: 45.34000
• Density: 1.1
• LogP: 3.95640

Purity/Quality:

95% ^*data from raw suppliers

DIETHYL 3-METHYLCYCLOHEX-1-ENYLPHOSPHONATE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 37/39-26

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of DIETHYL 3-METHYLCYCLOHEX-1-ENYLPHOSPHONATE

There total 1 articles about DIETHYL 3-METHYLCYCLOHEX-1-ENYLPHOSPHONATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

cyclohexenone (930-68-7) + diethyl chlorophosphate (814-49-3) → 3-Methyl-1-<(diethoxyphosphinyl)oxy>-1-cyclohexene (126424-00-8)

Guidance literature:

With triethylamine; Yield given. Multistep reaction; 1) ether, 1 h, rt, 2) 1.75 h, rt;

DOI:10.1021/jo00296a052

upstream raw materials:

cyclohexenone

diethyl chlorophosphate

Refernces