Disulfide, bis(4-methoxy-2-nitrophenyl)

Base Information

• Chemical Name: Disulfide, bis(4-methoxy-2-nitrophenyl)
• CAS No.: 14371-84-7
• Molecular Formula: C14H12 N2 O6 S2
• Molecular Weight: 368.391
• Hs Code.: 2930909090
• DSSTox Substance ID: DTXSID6065763
• Nikkaji Number: J421.917A
• Wikidata: Q81992379
• Mol file: 14371-84-7.mol

Synonyms:14371-84-7;Bis(2-nitro-4-methoxyphenyl)disulfide;Disulfide, bis(4-methoxy-2-nitrophenyl);4-methoxy-1-[(4-methoxy-2-nitrophenyl)disulfanyl]-2-nitrobenzene;di4-methoxy-2-nitrophenyl disulfide;SCHEMBL6516183;DTXSID6065763;AMY15527;MFCD00387458;STK396427;AKOS000567172;C14-H12-N2-O6-S2;Bis(4-methoxy-2-nitrophenyl) persulfide;3-Methoxy-1-nitrobenzene, 2,2'-dithiobis-;1,1'-disulfanediylbis(4-methoxy-2-nitrobenzene);4,4'-Dimethoxy-2,2'-dinitro-diphenyl-disulfid

Chemical Property of Disulfide, bis(4-methoxy-2-nitrophenyl)

Chemical Property:

• Vapor Pressure: 8.43E-11mmHg at 25°C
• Boiling Point: 530.4°C at 760 mmHg
• Flash Point: 274.6°C
• PSA: 160.70000
• Density: 1.5g/cm³
• LogP: 5.36600
• XLogP3: 3.3
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 8
• Rotatable Bond Count: 5
• Exact Mass: 368.01367845
• Heavy Atom Count: 24
• Complexity: 404

Purity/Quality:

98%Min ^*data from raw suppliers

BIS(2-NITRO-4-METHOXYPHENYL)DISULFIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: COC1=CC(=C(C=C1)SSC2=C(C=C(C=C2)OC)[N+](=O)[O-])[N+](=O)[O-]

Technology Process of Disulfide, bis(4-methoxy-2-nitrophenyl)

There total 7 articles about Disulfide, bis(4-methoxy-2-nitrophenyl) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

2-chloro-5-methoxynitrobenzene (10298-80-3) → 4,4′-dimethoxy-2,2′-dinitro-diphenyl disulfide (14371-84-7) + 4-methyl-2-nitrobenzenethiol (14371-80-3)

Guidance literature:

With sodium sulfide; In dimethyl sulfoxide; for 24h; Ambient temperature;

Reference yield: 35.0%

2-chloro-5-methoxynitrobenzene (10298-80-3) → 4,4′-dimethoxy-2,2′-dinitro-diphenyl disulfide (14371-84-7) + 4-Methoxy-2-nitro-benzenethiol (14371-81-4)

Guidance literature:

With sodium sulfide; In dimethyl sulfoxide; for 24h; Ambient temperature;

Reference yield:

2-chloro-5-methoxynitrobenzene (10298-80-3) → 4,4′-dimethoxy-2,2′-dinitro-diphenyl disulfide (14371-84-7)

Guidance literature:

With sodium disulfide; ethanol;

upstream raw materials:

4-bromo-3-nitroanizole

2-chloro-5-methoxynitrobenzene

2-nitro-4-methoxyphenyl thiocyanate

4-methoxy-2-nitroaniline

Downstream raw materials:

5-methoxy-2-methylbenzo[d]thiazole

5-methoxy-2-(4′-tolyl)benzo[d]thiazole

2-Nitro-4-methoxyphenylsulfenyl-DL-C-phenylglycin

2-Nitro-4-methoxyphenylsulfenyl-L-valin

Refernces