7-methoxy-1-methyl-1,2,3,7,8,9,10,11,12,12a-decahydro-7,10a-methano[1]benzoxocino[8,7,6-def]quinoline-5,8-diol

Base Information

• Chemical Name: 7-methoxy-1-methyl-1,2,3,7,8,9,10,11,12,12a-decahydro-7,10a-methano[1]benzoxocino[8,7,6-def]quinoline-5,8-diol
• CAS No.: 62624-08-2
• Molecular Formula: C₁₉H₂₅NO₄
• Molecular Weight: 331.4061
• Mol file: 62624-08-2.mol

Synonyms:O-Methyl-kesselringin;OMI;O-Methyl-isourea sulfate;2-Methyl-isourea sulfurate;Kesselringin;kesselringine;O-methyl-isourea hemisulfate;2-METHYLISO-UREASULFATE;OMISU;O-Methylisoharnstoffsulfat;O-METHYLPSEUDOUREA SULFATE;O-methylisourea hemisulphate;O-Methyluroniumsulfat;O-methylisourea hydrogen sulfate;methyl isourea,sulfate;

Chemical Property of 7-methoxy-1-methyl-1,2,3,7,8,9,10,11,12,12a-decahydro-7,10a-methano[1]benzoxocino[8,7,6-def]quinoline-5,8-diol

Chemical Property:

• Vapor Pressure: 7.99E-11mmHg at 25°C
• Boiling Point: 500.2°C at 760 mmHg
• Flash Point: 256.3°C
• PSA: 62.16000
• Density: 1.37g/cm³
• LogP: 2.17060

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 7-methoxy-1-methyl-1,2,3,7,8,9,10,11,12,12a-decahydro-7,10a-methano[1]benzoxocino[8,7,6-def]quinoline-5,8-diol

There total 5 articles about 7-methoxy-1-methyl-1,2,3,7,8,9,10,11,12,12a-decahydro-7,10a-methano[1]benzoxocino[8,7,6-def]quinoline-5,8-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

isoregelinone → luteine (54692-48-7,62624-08-2)

Guidance literature:

Multi-step reaction with 2 steps

1: Zn-dust / acetic acid / 4 h / Ambient temperature

2: Zn-dust, acetic acid / 8 h / Heating

With acetic acid; zinc; In acetic acid;

DOI:10.1007/BF00576216

Reference yield:

isoregecoline → luteine (54692-48-7,62624-08-2)

Guidance literature:

With acetic acid; zinc; for 8h; Heating;

DOI:10.1007/BF00576216

Reference yield:

12-demethylisoregecoline → luteine (54692-48-7,62624-08-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 7percent methanolic HCl / 1 h / Heating

2: Zn-dust, acetic acid / 8 h / Heating

With hydrogenchloride; acetic acid; zinc;

DOI:10.1007/BF00576216

upstream raw materials:

methanol

12-butoxy-kesselringane-2,11β-diol

12-propoxy-kesselringane-2,11β-diol

Refernces