Benzeneethanimidothioic acid, N-hydroxy-alpha-oxo-, phenyl ester

Base Information

Chemical Name:Benzeneethanimidothioic acid, N-hydroxy-alpha-oxo-, phenyl ester
CAS No.:110097-27-3
Molecular Formula:C14H11 N O2 S
Molecular Weight:257.3076
Hs Code.:

Synonyms:RA-59;2-Phenylthioglyoxilohydroximic acid S-phenyl ester;Glyoxilohydroximic acid, 2-phenylthio-, S-phenyl ester;Benzeneethanimidothioic acid, N-hydroxy-alpha-oxo-, phenyl ester;Benzeneethanimidothioicacid, N-hydroxy-a-oxo-, phenyl ester, (Z)-;110097-27-3;30822-65-2;LS-72995

Suppliers and Price of Benzeneethanimidothioic acid, N-hydroxy-alpha-oxo-, phenyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of Benzeneethanimidothioic acid, N-hydroxy-alpha-oxo-, phenyl ester

Chemical Property:

Vapor Pressure:0mmHg at 25°C
Boiling Point:443.9°Cat760mmHg
Flash Point:222.3°C
Density:1.19g/cm³
XLogP3:4.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:4
Exact Mass:257.05104977
Heavy Atom Count:18
Complexity:305

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C(=O)C(=NO)SC2=CC=CC=C2
Isomeric SMILES:C1=CC=C(C=C1)C(=O)/C(=N/O)/SC2=CC=CC=C2

Technology Process of Benzeneethanimidothioic acid, N-hydroxy-alpha-oxo-, phenyl ester

There total 2 articles about Benzeneethanimidothioic acid, N-hydroxy-alpha-oxo-, phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 108-98-5
thiophenol

: 614-21-1
2-nitroacetophenone

: 110097-27-3
(Z)-phenyl N-hydroxy-2-oxo-2-phenylethanimidothioate

Guidance literature:: With titanium tetrachloride; triethylamine; In tetrahydrofuran; at 25 ℃;
DOI:10.1021/jo00229a025

Reference yield:

: 10364-94-0
1-benzoylimidazole

: 110097-27-3
(Z)-phenyl N-hydroxy-2-oxo-2-phenylethanimidothioate

Guidance literature:: Multi-step reaction with 2 steps

1: 58 percent / tetrahydrofuran / 19 h / Heating

2: 60 percent / TiCl₄, Et₃N / tetrahydrofuran / 25 °C

With titanium tetrachloride; triethylamine; In tetrahydrofuran;
DOI:10.1021/jo00229a025