BLASTMYCETINA

Base Information

• Chemical Name: BLASTMYCETINA
• CAS No.: 107783-16-4
• Molecular Formula: C₃₅H₄₆N₆O₄
• Molecular Weight: 614.788
• Mol file: 107783-16-4.mol

Synonyms:3H-Pyrrolo[4,3,2-gh]-1,4-benzodiazonin-3-one,9,9'-methylenebis[1,2,4,5,6,8-hexahydro-5-(hydroxymethyl)-1-methyl-2-(1-methylethyl)-,[2S-[2R*,5R*,9(2'R*,5'R*)]]-; Blastmycetin A

Chemical Property of BLASTMYCETINA

Chemical Property:

• PSA: 0.00000
• LogP: 0.00000

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of BLASTMYCETINA

There total 5 articles about BLASTMYCETINA which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.2%

formaldehyd (50-00-0,30525-89-4,61233-19-0) + indolactam V (84590-48-7,84622-58-2,90365-54-1,90365-55-2,90365-56-3,132341-58-3,90365-57-4) → blastmycetin A (107783-16-4)

Guidance literature:

With methanol; In water; at 90 ℃; for 13h;

DOI:10.1271/bbb1961.52.641

Reference yield:

Blastmycetin B (107745-57-3) → blastmycetin A (107783-16-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) NaBH₄, 2.) LiAlH₄ / 1.) PdCl₂ / 1.) room temperature, 1.5 h; 2.) CH₂Cl₂, Et₂O, ultrasonication, 5 h

2: 45.2 percent / 10percent MeOH / H₂O / 13 h / 90 °C

With methanol; sodium tetrahydroborate; lithium aluminium tetrahydride; palladium dichloride; In water;

DOI:10.1271/bbb1961.52.641

Reference yield:

(-)-2-oxy-indolactam V → blastmycetin A (107783-16-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 6.2 percent / LiAlH₄ / 20 h / ultrasonication

2: 45.2 percent / 10percent MeOH / H₂O / 13 h / 90 °C

With methanol; lithium aluminium tetrahydride; In water;

DOI:10.1271/bbb1961.52.641

upstream raw materials:

formaldehyd

indolactam V

Blastmycetin C

Blastmycetin B