3-Butyl-3-azabicyclo[3.2.0]heptane-2,4-dione

Base Information

Chemical Name:3-Butyl-3-azabicyclo[3.2.0]heptane-2,4-dione
CAS No.:100131-99-5
Molecular Formula:C10H15NO2
Molecular Weight:181.235
Hs Code.:
DSSTox Substance ID:DTXSID70548565
Mol file:100131-99-5.mol

Synonyms:100131-99-5;3-BUTYL-3-AZABICYCLO[3.2.0]HEPTANE-2,4-DIONE;DTXSID70548565

Suppliers and Price of 3-Butyl-3-azabicyclo[3.2.0]heptane-2,4-dione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 3-Butyl-3-azabicyclo[3.2.0]heptane-2,4-dione

Chemical Property:

XLogP3:1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:181.110278721
Heavy Atom Count:13
Complexity:227

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCCN1C(=O)C2CCC2C1=O

Technology Process of 3-Butyl-3-azabicyclo[3.2.0]heptane-2,4-dione

There total 1 articles about 3-Butyl-3-azabicyclo[3.2.0]heptane-2,4-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4462-96-8
cis-1,2-cyclobutane dicarboxylic anhydride

: 109-73-9,85404-21-3
N-butylamine

: 100131-99-5
3-butyl-3-aza-bicyclo[3.2.0]heptane-2,4-dione

Guidance literature:: Erhitzen des Reaktionsgemisches auf 180grad;
DOI:10.1021/jo01360a029

Reference yield:

: 100131-99-5
3-butyl-3-aza-bicyclo[3.2.0]heptane-2,4-dione

: 111373-51-4,111956-87-7
(2aR,2bS,4S,6aS)-4-Phenyl-octahydro-5-oxa-5a-aza-cyclobuta[a]pentalene

Guidance literature:: Multi-step reaction with 4 steps

1: 92 percent / LiAlH₄

2: 1. MCPBA, 2. Cope elimination, 170 gradC

3: HgO

4: toluene / 110 °C

With lithium aluminium tetrahydride; mercury(II) oxide; In toluene;
DOI:10.1016/S0040-4039(00)95703-4

Reference yield:

: 100131-99-5
3-butyl-3-aza-bicyclo[3.2.0]heptane-2,4-dione

: Benzoic acid (2aR,2bS,4R,6aS)-4-(octahydro-5-oxa-5a-aza-cyclobuta[a]pentalen-4-yl)-butyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 92 percent / LiAlH₄

2: 1. MCPBA, 2. Cope elimination, 170 gradC

3: HgO

4: 64 percent / toluene / 80 °C / 2327170 Torr

With lithium aluminium tetrahydride; mercury(II) oxide; In toluene;
DOI:10.1016/S0040-4039(00)95703-4