Trimethyl[4-(trifluoromethyl)phenyl]germane

Base Information

Chemical Name:Trimethyl[4-(trifluoromethyl)phenyl]germane
CAS No.:100784-63-2
Molecular Formula:C₁₀H₁₃F₃Ge
Molecular Weight:262.798
Hs Code.:
DSSTox Substance ID:DTXSID30547135
Wikidata:Q82425171
Mol file:100784-63-2.mol

Synonyms:100784-63-2;Trimethyl[4-(trifluoromethyl)phenyl]germane;DTXSID30547135;InChI=1/C10H13F3Ge/c1-14(2,3)9-6-4-8(5-7-9)10(11,12)13/h4-7H,1-3H

Suppliers and Price of Trimethyl[4-(trifluoromethyl)phenyl]germane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Trimethyl[4-(trifluoromethyl)phenyl]germane

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:264.0181127
Heavy Atom Count:14
Complexity:185

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C[Ge](C)(C)C1=CC=C(C=C1)C(F)(F)F

Technology Process of Trimethyl[4-(trifluoromethyl)phenyl]germane

There total 1 articles about Trimethyl[4-(trifluoromethyl)phenyl]germane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 402-43-7
p-trifluoromethylphenyl bromide

: 1529-47-1
chlorotrimethylgermane

: 100784-63-2
p-Me₃GeC₆H₄CF₃

Guidance literature:: With magnesium; methyl iodide; In tetrahydrofuran; THF soln. of ArBr was added dropwise to Mg metal, reaction was initiated with MeI, stirred for 2 h at 25°C under Ar, a soln. of Me3GeCl in THF was added dropwise, mixt. was refluxed for 2 h; cooled, treated with 5% aq. NH4Cl, extd. with CH2Cl2, ext. was washed with water, dried (Na2SO4), fractionated; elem. anal.;
DOI:10.1016/0022-328X(87)80344-3