5,5'-Dichloro-2,2'-bipyridine

Base Information

Chemical Name:5,5'-Dichloro-2,2'-bipyridine
CAS No.:100846-27-3
Molecular Formula:C10H6Cl2N2
Molecular Weight:225.07400
Hs Code.:
DSSTox Substance ID:DTXSID20544491
Nikkaji Number:J1.712.553B
Wikidata:Q82421601
Mol file:100846-27-3.mol

Synonyms:5,5'-DICHLORO-2,2'-BIPYRIDINE;100846-27-3;2,2'-Bipyridine, 5,5'-dichloro-;5-CHLORO-2-(5-CHLOROPYRIDIN-2-YL)PYRIDINE;SCHEMBL197456;DTXSID20544491;AKOS015944523;J-400677

Suppliers and Price of 5,5'-Dichloro-2,2'-bipyridine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
5,5'-DICHLORO-2,2'-BIPYRIDINE 95.00%
5MG
$ 499.98

Total 1 raw suppliers

Chemical Property of 5,5'-Dichloro-2,2'-bipyridine

Chemical Property:

Melting Point:199-200 °C
Boiling Point:320.573oC at 760 mmHg
PKA:1.59±0.32(Predicted)
Flash Point:177.243oC
PSA：25.78000
Density:1.364g/cm3
LogP:3.45040
XLogP3:2.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:223.9908036
Heavy Atom Count:14
Complexity:169

Purity/Quality:: 5,5'-DICHLORO-2,2'-BIPYRIDINE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=NC=C1Cl)C2=NC=C(C=C2)Cl

Technology Process of 5,5'-Dichloro-2,2'-bipyridine

There total 9 articles about 5,5'-Dichloro-2,2'-bipyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 40473-01-6
2-Bromo-5-chloro-pyridine

: 100846-27-3
5,5'-dichloro-2,2'-bipyridine

Guidance literature:: With nickel(II) chloride hexahydrate; iodine; acetic acid; lithium chloride; zinc; In N,N-dimethyl-formamide; at 50 - 60 ℃; for 6h;
DOI:10.1021/jo402084m

Reference yield: 49.0%

: 626-60-8
3-Chloropyridine

: 16663-57-3
3-chloropyridinetrifluoroborate

: 100846-27-3
5,5'-dichloro-2,2'-bipyridine

: 1478090-82-2
3,3’-dichloro-2,6’-bipyridine

Guidance literature:: 3-chloropyridinetrifluoroborate; With lithium diisopropyl amide; In diethyl ether; at -78 ℃; Inert atmosphere;

3-Chloropyridine; In diethyl ether; at -78 ℃; Inert atmosphere;

With water;
DOI:10.1016/j.tet.2013.10.026

Reference yield: 44.0%

: 16663-57-3
3-chloropyridinetrifluoroborate

: 100846-27-3
5,5'-dichloro-2,2'-bipyridine

: 1478090-82-2
3,3’-dichloro-2,6’-bipyridine

Guidance literature:: 3-chloropyridinetrifluoroborate; With lithium diisopropyl amide; In diethyl ether; at -78 ℃; Inert atmosphere;

With Dimethyldisulphide; In diethyl ether; Inert atmosphere;

With water;
DOI:10.1016/j.tet.2013.10.026