(E)-1-Phenyl-N-[5-(trimethylsilyl)pent-3-yn-1-yl]methanimine

Base Information

Chemical Name:(E)-1-Phenyl-N-[5-(trimethylsilyl)pent-3-yn-1-yl]methanimine
CAS No.:101195-69-1
Molecular Formula:C15H21NSi
Molecular Weight:243.424
Hs Code.:
DSSTox Substance ID:DTXSID60540679
Nikkaji Number:J2.222.071C
Mol file:101195-69-1.mol

Synonyms:101195-69-1;DTXSID60540679;(E)-1-Phenyl-N-[5-(trimethylsilyl)pent-3-yn-1-yl]methanimine

Suppliers and Price of (E)-1-Phenyl-N-[5-(trimethylsilyl)pent-3-yn-1-yl]methanimine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (E)-1-Phenyl-N-[5-(trimethylsilyl)pent-3-yn-1-yl]methanimine

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:4
Exact Mass:243.144326209
Heavy Atom Count:17
Complexity:294

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C[Si](C)(C)CC#CCCN=CC1=CC=CC=C1

Technology Process of (E)-1-Phenyl-N-[5-(trimethylsilyl)pent-3-yn-1-yl]methanimine

There total 4 articles about (E)-1-Phenyl-N-[5-(trimethylsilyl)pent-3-yn-1-yl]methanimine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 101195-67-9
5-Trimethylsilanyl-pent-3-ynylamine

: 100-52-7
benzaldehyde

: 101195-69-1
[1-Phenyl-meth-(E)-ylidene]-(5-trimethylsilanyl-pent-3-ynyl)-amine

Guidance literature:: In toluene; Ambient temperature;
DOI:10.1016/S0040-4039(00)98643-X

Reference yield:

: 108634-59-9
Methanesulfonic acid 5-trimethylsilanyl-pent-3-ynyl ester

: 101195-69-1
[1-Phenyl-meth-(E)-ylidene]-(5-trimethylsilanyl-pent-3-ynyl)-amine

Guidance literature:: Multi-step reaction with 3 steps

1: NaN₃ / dimethylformamide / 1.5 h / 110 °C

2: 1.) PPh₃; 2.) H₂O / 1.) THF, 2 h; 2.) 16 h

3: toluene / Ambient temperature

With sodium azide; water; triphenylphosphine; In N,N-dimethyl-formamide; toluene;
DOI:10.1016/S0040-4039(00)98643-X

Reference yield:

: 86486-02-4
1-(Trimethylsilyl)-2-pentyn-5-ol

: 101195-69-1
[1-Phenyl-meth-(E)-ylidene]-(5-trimethylsilanyl-pent-3-ynyl)-amine

Guidance literature:: Multi-step reaction with 4 steps

1: Et₃N / CH₂Cl₂ / 0 - 20 °C

2: NaN₃ / dimethylformamide / 1.5 h / 110 °C

3: 1.) PPh₃; 2.) H₂O / 1.) THF, 2 h; 2.) 16 h

4: toluene / Ambient temperature

With sodium azide; water; triethylamine; triphenylphosphine; In dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1016/S0040-4039(00)98643-X