Benzylquinolone

Base Information

Chemical Name:Benzylquinolone
CAS No.:101273-50-1
Molecular Formula:C₁₆H₁₃NO
Molecular Weight:235.285
Hs Code.:
DSSTox Substance ID:DTXSID90479367
Nikkaji Number:J2.143.172I
Wikidata:Q82313362
Mol file:101273-50-1.mol

Synonyms:benzylquinolone;DTXSID90479367

Suppliers and Price of Benzylquinolone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Benzylquinolone

Chemical Property:

XLogP3:3.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:235.099714038
Heavy Atom Count:18
Complexity:341

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)CC2=CC3=CC=CC=C3NC2=O

Technology Process of Benzylquinolone

There total 6 articles about Benzylquinolone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 59-31-4
2-hydroxyquinoline

: 100-51-6,185532-71-2
benzyl alcohol

: 101273-50-1
3-benzylquinolin-2-ol

Guidance literature:: With potassium hydroxide; unter Entfernen des entstehenden Wassers;
DOI:10.1021/ja01597a063

Reference yield:

: 124957-36-4
Methyl 3-acetoxy-2-methylene-3-phenylpropanoate

: 101273-50-1
3-benzylquinolin-2-ol

Guidance literature:: Multi-step reaction with 3 steps

1.1: DABCO / tetrahydrofuran; H₂O / 0.5 h

1.2: 87 percent / 18 h / 20 °C

2.1: 79 percent / polyphosphoric acid / 7 h / 80 - 90 °C

3.1: 93 percent / DBU / tetrahydrofuran / 1 h / 20 °C

With 1,4-diaza-bicyclo[2.2.2]octane; PPA; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; water;
DOI:10.1016/j.tet.2004.11.082

Reference yield:

: 137104-49-5
methyl 2-<α-(phenylamino)benzyl>prop-2-enoate

: 101273-50-1
3-benzylquinolin-2-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / polyphosphoric acid / 7 h / 80 - 90 °C

2: 93 percent / DBU / tetrahydrofuran / 1 h / 20 °C

With PPA; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran;
DOI:10.1016/j.tet.2004.11.082