Benzoic acid, 3,4-dimethoxy-5-(phenylmethoxy)-, hydrazide

Base Information

Chemical Name:Benzoic acid, 3,4-dimethoxy-5-(phenylmethoxy)-, hydrazide
CAS No.:101289-41-2
Molecular Formula:C16H18N2O4
Molecular Weight:302.32500
Hs Code.:
European Community (EC) Number:651-906-3
DSSTox Substance ID:DTXSID00402161
Wikidata:Q82205535

Synonyms:101289-41-2;Benzoic acid, 3,4-dimethoxy-5-(phenylmethoxy)-, hydrazide;3-BENZYLOXY-4,5-DIMETHOXY-BENZOIC ACID HYDRAZIDE;DTXSID00402161;AKOS024330598

Suppliers and Price of Benzoic acid, 3,4-dimethoxy-5-(phenylmethoxy)-, hydrazide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Benzoic acid, 3,4-dimethoxy-5-(phenylmethoxy)-, hydrazide

Chemical Property:

PSA：86.30000
LogP:3.16140
XLogP3:1.9
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:6
Exact Mass:302.12665706
Heavy Atom Count:22
Complexity:347

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=C(C(=CC(=C1)C(=O)NN)OCC2=CC=CC=C2)OC

Technology Process of Benzoic acid, 3,4-dimethoxy-5-(phenylmethoxy)-, hydrazide

There total 5 articles about Benzoic acid, 3,4-dimethoxy-5-(phenylmethoxy)-, hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 26409-24-5
methyl 3-benzyloxy-4,5-dimethoxybenzoate

: 101289-41-2
3-benzyloxy-4,5-dihydroxybenzoic acid hydrazide

Guidance literature:: With hydrazine hydrate; In ethanol; for 18h; Heating;

Reference yield:

: 79831-86-0
methyl 3-(benzyloxy)-4,5-dihydroxybenzoate

: 101289-41-2
3-benzyloxy-4,5-dihydroxybenzoic acid hydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / acetone / 3 h / Heating

2: 19.5 g / hydrazine dihydrate / ethanol / 12 h / Heating

With potassium carbonate; hydrazine hydrate; In ethanol; acetone;
DOI:10.1039/P19810002016

Reference yield:

: 99-24-1
methyl galloate

: 101289-41-2
3-benzyloxy-4,5-dihydroxybenzoic acid hydrazide

Guidance literature:: Multi-step reaction with 3 steps

1: 29 percent / potassium carbonate, borax / dimethylformamide; H₂O / 29 h

2: 92 percent / potassium carbonate / acetone / 72 h / Heating

3: 94 percent / hydrazinum hydroxide / ethanol / 18 h / Heating

With borax; potassium carbonate; hydrazine hydrate; In ethanol; water; N,N-dimethyl-formamide; acetone;