{4-[5-(1,3-Dioxan-2-yl)-2-methoxyphenoxy]phenyl}methanol

Base Information

Chemical Name:{4-[5-(1,3-Dioxan-2-yl)-2-methoxyphenoxy]phenyl}methanol
CAS No.:101553-98-4
Molecular Formula:C18H20O5
Molecular Weight:316.354
Hs Code.:
DSSTox Substance ID:DTXSID20554358
Nikkaji Number:J2.907.648K
Wikidata:Q82435318
Mol file:101553-98-4.mol

Synonyms:101553-98-4;DTXSID20554358;{4-[5-(1,3-Dioxan-2-yl)-2-methoxyphenoxy]phenyl}methanol

Suppliers and Price of {4-[5-(1,3-Dioxan-2-yl)-2-methoxyphenoxy]phenyl}methanol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 1 raw suppliers

Chemical Property of {4-[5-(1,3-Dioxan-2-yl)-2-methoxyphenoxy]phenyl}methanol

Chemical Property:

XLogP3:2.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:5
Exact Mass:316.13107373
Heavy Atom Count:23
Complexity:336

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COC1=C(C=C(C=C1)C2OCCCO2)OC3=CC=C(C=C3)CO

Technology Process of {4-[5-(1,3-Dioxan-2-yl)-2-methoxyphenoxy]phenyl}methanol

There total 6 articles about {4-[5-(1,3-Dioxan-2-yl)-2-methoxyphenoxy]phenyl}methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1186304-19-7
4-[5-(1,3-dioxan-2-yl)-2-methoxyphenoxy]benzaldehyde

: 101553-98-4
{4-[5-(1,3-dioxan-2-yl)-2-methoxyphenoxy]phenyl}methanol

Guidance literature:: With sodium tetrahydroborate; In ethanol; at 0 - 20 ℃; for 2h;
DOI:10.1055/s-0029-1217510

Reference yield: 77.0%

: 111436-60-3
methyl 4-<2-methoxy-5-(1,3-dioxan-2-yl)phenoxy>benzoate

: 101553-98-4
{4-[5-(1,3-dioxan-2-yl)-2-methoxyphenoxy]phenyl}methanol

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; Ambient temperature;
DOI:10.1021/jo00236a015

Reference yield:

: 621-59-0
isovanillin

: 101553-98-4
{4-[5-(1,3-dioxan-2-yl)-2-methoxyphenoxy]phenyl}methanol

Guidance literature:: Multi-step reaction with 3 steps

1: 79 percent / K₂CO₃-CuO / pyridine / Heating

2: p-TsOH

3: LiAlH₄

With lithium aluminium tetrahydride; potassium carbonate; copper(II) oxide; toluene-4-sulfonic acid; In pyridine;
DOI:10.1246/cl.1985.1587