N-phenyldihydroquinolinone 1-phenyl-2,3-dihydro-1H-quinolin-4-one

Base Information

• Chemical Name: N-phenyldihydroquinolinone 1-phenyl-2,3-dihydro-1H-quinolin-4-one
• CAS No.: 10258-13-6
• Molecular Formula: C15H13NO
• Molecular Weight: 223.274
• Mol file: 10258-13-6.mol

Synonyms:1-Phenyl-2,3-dihydro-1H-quinolin-4-one;1-Phenyl-2,3-dihydro-1H-chinolin-4-on;2,3-dihydro-1-phenyl-4(1H)-quinolone;

Chemical Property of N-phenyldihydroquinolinone 1-phenyl-2,3-dihydro-1H-quinolin-4-one

Chemical Property:

• PSA: 20.31000
• LogP: 3.47610

Purity/Quality:

97% ^*data from raw suppliers

1-Phenyl-2,3-dihydro-1H-quinolin-4-one ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N-phenyldihydroquinolinone 1-phenyl-2,3-dihydro-1H-quinolin-4-one

There total 13 articles about N-phenyldihydroquinolinone 1-phenyl-2,3-dihydro-1H-quinolin-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

2,3-dihydroquinolin-4(1H)-one (4295-36-7) + 2-(trimethylsilyl)phenyl trifluoromethanesulfonate (88284-48-4) → 1-phenyl-2,3-dihydro-1H-quinolin-4-one (10258-13-6) + 10-phenylacridin-9(10H)-one (5472-23-1)

Guidance literature:

With cesium fluoride; In acetonitrile; at 23 ℃; for 2h;

DOI:10.1016/j.tetlet.2012.07.026

Reference yield: 32.0%

diphenylamine (122-39-4) + acrylic acid methyl ester (292638-85-8,9003-21-8,96-33-3) → 1-phenyl-2,3-dihydro-1H-quinolin-4-one (10258-13-6)

Guidance literature:

With copper(l) iodide; trifluorormethanesulfonic acid; trifluoromethylsulfonic anhydride; In 1,2-dichloro-ethane; at 120 ℃; for 24h;

DOI:10.1021/acs.orglett.8b00436

Reference yield: 31.0%

2-azetidinone (930-21-2) + 2-(trimethylsilyl)phenyl trifluoromethanesulfonate (88284-48-4) → 1-phenyl-2,3-dihydro-1H-quinolin-4-one (10258-13-6) + 10-phenylacridin-9(10H)-one (5472-23-1)

Guidance literature:

With potassium fluoride; 18-crown-6 ether; In tetrahydrofuran; at 23 ℃; for 2h;

DOI:10.1016/j.tetlet.2012.07.026

upstream raw materials:

N,N-diphenyl-β-alanine

N,N-Dimethylacrylamide

diphenylamine

carbon disulfide

Downstream raw materials:

3-[2]quinolylmethylene-1-phenyl-2,3-dihydro-1H-quinolin-4-one

3-(4-dimethylamino-benzylidene)-1-phenyl-2,3-dihydro-1H-quinolin-4-one

3-(4-dimethylamino-anilino)-1-phenyl-1H-quinolin-4-one

(1-phenyl-2,3-dihydro-1H-[4]chinolyLiDene)-malononitrile

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