Silacycloprop-2-ene, 2-phenyl-1-(2,4,6-trimethylphenyl)-1,3-bis(trimethylsilyl)-

Base Information

Chemical Name:Silacycloprop-2-ene, 2-phenyl-1-(2,4,6-trimethylphenyl)-1,3-bis(trimethylsilyl)-
CAS No.:102632-48-4
Molecular Formula:C23H34Si3
Molecular Weight:394.779
Hs Code.:
Mol file:102632-48-4.mol

Synonyms:

Suppliers and Price of Silacycloprop-2-ene, 2-phenyl-1-(2,4,6-trimethylphenyl)-1,3-bis(trimethylsilyl)-

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Silacycloprop-2-ene, 2-phenyl-1-(2,4,6-trimethylphenyl)-1,3-bis(trimethylsilyl)-

Chemical Property:

Purity/Quality:

Safty Information:

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Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of Silacycloprop-2-ene, 2-phenyl-1-(2,4,6-trimethylphenyl)-1,3-bis(trimethylsilyl)-

There total 4 articles about Silacycloprop-2-ene, 2-phenyl-1-(2,4,6-trimethylphenyl)-1,3-bis(trimethylsilyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 100-39-0
benzyl bromide

: 2-mesityl-4-phenyl-1,1-bis(triethylphosphine)-2,3-bis(trimethylsilyl)-1-nickela-2-silacyclobut-3-ene

: 102632-48-4
1-mesityl-3-phenyl-1,2-bis(trimethylsilyl)-1-silacyclopropene

: 103-29-7
1,1'-(1,2-ethanediyl)bisbenzene

Guidance literature:: In xylene; byproducts: (Et3P)2NiBr2; addn. of benzyl bromide to a mixt. of the Ni compd. and eicosane (as internal standard) in xylol under Ar (ice cooling), stirring (room temp., 12 h); isolation by medium-pressure liquid chromy.;
DOI:10.1021/om00110a036

Reference yield: 100.0%

: 2-mesityl-4-phenyl-1,1-bis(triethylphosphine)-2,3-bis(trimethylsilyl)-1-nickela-2-silacyclobut-3-ene

: 102632-48-4
1-mesityl-3-phenyl-1,2-bis(trimethylsilyl)-1-silacyclopropene

Guidance literature:: With bromine; In xylene; byproducts: (Et3P)2NiBr2; addn. of bromine to a mixt. of the Ni compd. and eicosane (as internal standard) in xylol under Ar (ice cooling), stirring (30 min); anal. by VPC;
DOI:10.1021/om00110a036