Technology Process of 2-Cyclohexene-1-acetyl chloride, 1-ethyl-
There total 2 articles about 2-Cyclohexene-1-acetyl chloride, 1-ethyl- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
oxalyl dichloride;
In
dichloromethane;
for 2h;
Heating;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 94.4 percent / aq. KOH / methanol / 2 h / Heating
2: 88.6 percent / oxalyl chloride / CH2Cl2 / 2 h / Heating
With
potassium hydroxide; oxalyl dichloride;
In
methanol; dichloromethane;
-
-
103557-92-2,142560-76-7
benzyl N-<(3aα,12α,12aα,12bα)-1,2,3,3a,4,5,11,12,12a,12b-decahydro-3aα-ethyl-5-oxoisoquino<2,1,8-lma>carbazol-12-yl>carbamate
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 1.) NaH / 1.) DMF, RT, 30 min, 2.) DMF, 0.5 h
2: 74.6 percent / 1,3,5-trimethyl-benzene / 20 h / Heating
3: 97.7 percent / HCl / ethanol; dioxane / 0.5 h / Heating
4: 89.6 percent / aq. KOH / methanol / 0.5 h / Heating
5: diphenylphosphoryl azide, triethylamine / toluene / 1 h / Heating
6: toluene / 2 h / Heating
With
hydrogenchloride; potassium hydroxide; diphenylphosphoranyl azide; sodium hydride; triethylamine;
In
1,4-dioxane; methanol; ethanol; toluene; 1,3,5-trimethyl-benzene;
