Stannane, tributyl(1-phenyl-2-propenyl)-

Base Information

Chemical Name:Stannane, tributyl(1-phenyl-2-propenyl)-
CAS No.:104108-28-3
Molecular Formula:C₂₁H₃₆Sn
Molecular Weight:407.227
Hs Code.:
DSSTox Substance ID:DTXSID70466371
Mol file:104108-28-3.mol

Synonyms:Stannane, tributyl(1-phenyl-2-propenyl)-;104108-28-3;DTXSID70466371

Suppliers and Price of Stannane, tributyl(1-phenyl-2-propenyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Stannane, tributyl(1-phenyl-2-propenyl)-

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:12
Exact Mass:408.183904
Heavy Atom Count:22
Complexity:256

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCC[Sn](CCCC)(CCCC)C(C=C)C1=CC=CC=C1

Technology Process of Stannane, tributyl(1-phenyl-2-propenyl)-

There total 13 articles about Stannane, tributyl(1-phenyl-2-propenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: bis(tributylstannyl)lithium(cuprate)

: 2327-99-3
1-phenylpropadiene

: 124582-43-0,131428-21-2
(C₆H₅)C(H)C(CH₃)(tributylstannyl)

: 19752-27-3,104108-28-3
phenylallyl(tributyl)stannane

Guidance literature:: With ammonium chloride; In tetrahydrofuran; React. of starting materials (THF, -78 to 0°C, 1 h).;
DOI:10.1039/c39900001030

Reference yield: 84.0%

: 17955-46-3
trimethylsilyltributyltin

: 77821-95-5
3-phenyl-2-propen-1-yl 2,2-dimethylproponate

: 19752-27-3,104108-28-3
phenylallyl(tributyl)stannane

Guidance literature:: With bis(1,5-cyclooctadiene)nickel ⁽⁰⁾; cesium fluoride; 1,2-bis-(dicyclohexylphosphino)ethane; In toluene; at 90 ℃; for 8h; Inert atmosphere; Sealed tube;
DOI:10.1002/anie.201611720

Reference yield: 81.0%

: 68725-14-4
tri-n-butyltin triflate

: 19752-27-3,104108-28-3
phenylallyl(tributyl)stannane

Guidance literature:: With phenylpropenyllithium; In tetrahydrofuran; react. of Li- and tin-compd. initially at -78°C, then up to 23°C over 10 min;
DOI:10.1021/ja00260a039