1-Ethynyl-4-methylcyclohex-1-ene

Base Information

Chemical Name:1-Ethynyl-4-methylcyclohex-1-ene
CAS No.:104258-28-8
Molecular Formula:C9H12
Molecular Weight:120.194
Hs Code.:
DSSTox Substance ID:DTXSID90543259
Mol file:104258-28-8.mol

Synonyms:104258-28-8;1-Ethynyl-4-methylcyclohex-1-ene;DTXSID90543259

Suppliers and Price of 1-Ethynyl-4-methylcyclohex-1-ene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 1-Ethynyl-4-methylcyclohex-1-ene

Chemical Property:

XLogP3:2.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:1
Exact Mass:120.093900383
Heavy Atom Count:9
Complexity:166

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1CCC(=CC1)C#C

Technology Process of 1-Ethynyl-4-methylcyclohex-1-ene

There total 3 articles about 1-Ethynyl-4-methylcyclohex-1-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 119472-66-1
4-methylcyclohex-1-en-1-yl trifluoromethanesulfonate

: 4301-14-8
acetylenemagnesium bromide

: 104258-28-8
1-ethynyl-4-methylcyclohex-1-ene

Guidance literature:: With cobalt(III) acetylacetonate; In tetrahydrofuran; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1021/ja405043g

Reference yield:

: 589-92-4
1-methylcyclohexan-4-one

: 104258-28-8
1-ethynyl-4-methylcyclohex-1-ene

Guidance literature:: Multi-step reaction with 2 steps

1: liquid NH₃; diethyl ether

2: 300 - 310 °C / Leiten ueber AlPO₄ auf poroesem Traeger

With diethyl ether; ammonia;