1-[(Phenylsulfanyl)methyl]cyclohept-1-ene

Base Information

Chemical Name:1-[(Phenylsulfanyl)methyl]cyclohept-1-ene
CAS No.:104281-70-1
Molecular Formula:C14H18S
Molecular Weight:218.363
Hs Code.:
DSSTox Substance ID:DTXSID40543441
Nikkaji Number:J508.731G
Mol file:104281-70-1.mol

Synonyms:104281-70-1;1-[(Phenylsulfanyl)methyl]cyclohept-1-ene;DTXSID40543441

Suppliers and Price of 1-[(Phenylsulfanyl)methyl]cyclohept-1-ene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-[(Phenylsulfanyl)methyl]cyclohept-1-ene

Chemical Property:

XLogP3:4.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:218.11292175
Heavy Atom Count:15
Complexity:201

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CCC=C(CC1)CSC2=CC=CC=C2

Technology Process of 1-[(Phenylsulfanyl)methyl]cyclohept-1-ene

There total 14 articles about 1-[(Phenylsulfanyl)methyl]cyclohept-1-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 101704-20-5
1-(phenylthiomethyl)cycloheptanol

: 104281-70-1
1-cycloheptenylmethyl phenyl sulfide

Guidance literature:: With toluene-4-sulfonic acid; In benzene; for 7h; Heating;
DOI:10.1055/s-1987-28081

Reference yield:

: 104281-74-5
2-Phenylthio-2-(trimethylsilylmethyl)cycloheptanone

: 104281-70-1
1-cycloheptenylmethyl phenyl sulfide

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / LiAlH₄ / diethyl ether / 0 °C

2: TsOH

3: Irradiation; other exo allylic sulfides

With lithium aluminium tetrahydride; toluene-4-sulfonic acid; In diethyl ether;

Reference yield:

: 931-59-9
benzenesulfenyl chloride

: 104281-70-1
1-cycloheptenylmethyl phenyl sulfide

Guidance literature:: Multi-step reaction with 4 steps

2: LiAlH₄

3: TsOH / benzene / Heating

4: Irradiation

With lithium aluminium tetrahydride; toluene-4-sulfonic acid; In benzene;
DOI:10.1016/S0040-4039(00)84095-2