Dithiodiglycolic acid dihydrazide

Base Information

• Chemical Name: Dithiodiglycolic acid dihydrazide
• CAS No.: 6854-84-8
• Molecular Formula: C4H10N4O2S2
• Molecular Weight: 210.281
• NSC Number: 209418
• DSSTox Substance ID: DTXSID10218659
• Wikidata: Q83095551

Synonyms:Dithiodiglycolic acid dihydrazide;6854-84-8;Acethydrazide disulfide;Dithiodiacetyl dihydrazide;Dithioglycollic dihydrazide;2,2'-Dithiobisacetic acid dihydrazide;NSC 209418;BRN 1788647;Acetic acid, 2,2'-dithiobis-, dihydrazide;2,2'-Disulfanediyldi(acetohydrazide);ACETIC ACID, DITHIODI-, DIHYDRAZIDE;4-03-00-00632 (Beilstein Handbook Reference);Acetic acid, 2,2'-dithiobis-, dihydrazide (9CI);2-[(2-hydrazinyl-2-oxoethyl)disulfanyl]acetohydrazide;SCHEMBL13302372;C4H10N4O2S2;DTXSID10218659;C4-H10-N4-O2-S2;NSC209418;NSC-209418;Acetic acid, 2,2'-dithiobis-dihydrazide

Chemical Property of Dithiodiglycolic acid dihydrazide

Chemical Property:

• XLogP3: -1.9
• Hydrogen Bond Donor Count: 4
• Hydrogen Bond Acceptor Count: 6
• Rotatable Bond Count: 5
• Exact Mass: 210.02451792
• Heavy Atom Count: 12
• Complexity: 147

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C(C(=O)NN)SSCC(=O)NN

Technology Process of Dithiodiglycolic acid dihydrazide

There total 11 articles about Dithiodiglycolic acid dihydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

2-mercaptoacetohydrazide (760-30-5) + Dithiophosphoric acid S-chlorocarbonylmethyl ester O,O'-dipropyl ester → 2,2′-disulfanediyldi(acetohydrazide) (6854-84-8) + (Dipropoxy-thiophosphorylsulfanyl)-thioacetic acid S-hydrazinocarbonylmethyl ester + Dithiophosphoric acid S-(2-{N'-[2-(dipropoxy-thiophosphorylsulfanyl)-acetyl]-hydrazino}-2-oxo-ethyl) ester O,O'-dipropyl ester + (Dipropoxy-thiophosphorylsulfanyl)-acetic acid; compound with hydrazinocarbonylmethyldisulfanyl-acetic acid hydrazide

Guidance literature:

With triethylamine; In 1,4-dioxane; at 50 ℃;

Reference yield: 66.0%

2-mercaptoacetohydrazide (760-30-5) + O,O-Diaethyl-S-chlor-formylmethyl-dithiophosphat (2047-15-6) → 2,2′-disulfanediyldi(acetohydrazide) (6854-84-8) + (Diethoxy-thiophosphorylsulfanyl)-thioacetic acid S-hydrazinocarbonylmethyl ester + Dithiophosphoric acid S-{N'-[2-(diethoxy-thiophosphorylsulfanyl)-acetyl]-hydrazinocarbonylmethyl} ester O,O'-diethyl ester + (Diethoxy-thiophosphorylsulfanyl)-acetic acid; compound with hydrazinocarbonylmethyldisulfanyl-acetic acid hydrazide

Guidance literature:

With triethylamine; In 1,4-dioxane; at 50 ℃;

Reference yield: 63.0%

2-mercaptoacetohydrazide (760-30-5) + Dithiophosphoric acid S-chlorocarbonylmethyl ester O,O'-diisobutyl ester → 2,2′-disulfanediyldi(acetohydrazide) (6854-84-8) + (Diisobutoxy-thiophosphorylsulfanyl)-thioacetic acid S-hydrazinocarbonylmethyl ester + Dithiophosphoric acid S-(2-{N'-[2-(diisobutoxy-thiophosphorylsulfanyl)-acetyl]-hydrazino}-2-oxo-ethyl) ester O,O'-diisobutyl ester + (Diisobutoxy-thiophosphorylsulfanyl)-acetic acid; compound with hydrazinocarbonylmethyldisulfanyl-acetic acid hydrazide

Guidance literature:

With triethylamine; In 1,4-dioxane; at 50 ℃;

upstream raw materials:

2-mercaptoacetohydrazide

O,O-Diaethyl-S-chlor-formylmethyl-dithiophosphat

O,O-diethyl-S-(2-chlorocarbonylethyl)dithiophosphate

Dithiophosphoric acid S-(2-chlorocarbonyl-ethyl) ester O,O'-diisopropyl ester

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