1-(1-Chloropropane-1-sulfonyl)-4-methylbenzene

Base Information

Chemical Name:1-(1-Chloropropane-1-sulfonyl)-4-methylbenzene
CAS No.:105199-35-7
Molecular Formula:C10H13ClO2S
Molecular Weight:232.72700
Hs Code.:
DSSTox Substance ID:DTXSID00550191
Mol file:105199-35-7.mol

Synonyms:105199-35-7;1-(1-Chloropropane-1-sulfonyl)-4-methylbenzene;DTXSID00550191

Suppliers and Price of 1-(1-Chloropropane-1-sulfonyl)-4-methylbenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 1-(1-Chloropropane-1-sulfonyl)-4-methylbenzene

Chemical Property:

Melting Point:74-75 °C(Solv: ethanol (64-17-5))
Boiling Point:361.3±42.0 °C(Predicted)
PSA：42.52000
Density:1.210±0.06 g/cm3(Predicted)
LogP:3.82440
XLogP3:3.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:232.0324785
Heavy Atom Count:14
Complexity:260

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCC(S(=O)(=O)C1=CC=C(C=C1)C)Cl

Technology Process of 1-(1-Chloropropane-1-sulfonyl)-4-methylbenzene

There total 4 articles about 1-(1-Chloropropane-1-sulfonyl)-4-methylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 925901-20-8
2-chloro-1-phenyl-2-(toluene-4-sulfonyl)-butan-1-one

: 105199-35-7
α-Chloropropyl p-Tolyl Sulfone

Guidance literature:: With sodium hydroxide; at 20 ℃; for 0.5h;
DOI:10.1016/j.tetlet.2006.11.129

Reference yield: 85.0%

: 74-96-4
ethyl bromide

: 7569-26-8
chloromethyl p-tolylsulfone

: 105199-35-7
α-Chloropropyl p-Tolyl Sulfone

Guidance literature:: With sodium hydroxide; tetrabutylammomium bromide; In benzene; at 40 ℃; for 4h;

Reference yield:

: 31378-03-7
1-phenyl-2-tosylethanone

: 105199-35-7
α-Chloropropyl p-Tolyl Sulfone

Guidance literature:: Multi-step reaction with 3 steps

1: K₂CO₃ / acetonitrile / 20 °C

2: 96 percent / KCl; hydrogen peroxide / acetone / 6 h / 20 °C

3: 99 percent / aq. NaOH / 0.5 h / 20 °C

With sodium hydroxide; potassium chloride; dihydrogen peroxide; potassium carbonate; In acetone; acetonitrile;
DOI:10.1016/j.tetlet.2006.11.129