Benzenesulfonic acid, 2,5-dichloro-, 2-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-1-[[[(1,1-dimethylethyl)dimethylsil yl]oxy]methyl]ethyl ester

Base Information

• Chemical Name: Benzenesulfonic acid, 2,5-dichloro-, 2-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-1-[[[(1,1-dimethylethyl)dimethylsil yl]oxy]methyl]ethyl ester
• CAS No.: 105376-71-4
• Molecular Formula: C21H38Cl2O5SSi2
• Molecular Weight: 529.673
• Mol file: 105376-71-4.mol

Synonyms:

Chemical Property of Benzenesulfonic acid, 2,5-dichloro-, 2-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-1-[[[(1,1-dimethylethyl)dimethylsil yl]oxy]methyl]ethyl ester

Chemical Property:

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MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzenesulfonic acid, 2,5-dichloro-, 2-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-1-[[[(1,1-dimethylethyl)dimethylsil yl]oxy]methyl]ethyl ester

There total 1 articles about Benzenesulfonic acid, 2,5-dichloro-, 2-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-1-[[[(1,1-dimethylethyl)dimethylsil yl]oxy]methyl]ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

tert-butyldimethylsilyl chloride (18162-48-6) + 2,5-Dichloro-benzenesulfonic acid 2-hydroxy-1-hydroxymethyl-ethyl ester → 1,3-Bis(t-butyldimethylsiloxy)prop-2-yl 2,5-dichlorobenzenesulphonate (105376-71-4)

Guidance literature:

With 1H-imidazole; In N,N-dimethyl-formamide;

DOI:10.1039/c39860000867

Reference yield: 95.0%

3,5-dichlorophenol (591-35-5) + 1,3-Bis(t-butyldimethylsiloxy)prop-2-yl 2,5-dichlorobenzenesulphonate (105376-71-4) → 1-[2-(tert-Butyl-dimethyl-silanyloxy)-1-(tert-butyl-dimethyl-silanyloxymethyl)-ethoxy]-3,5-dichloro-benzene

Guidance literature:

With 18-crown-6 ether; sodium hydride; In tetrahydrofuran; 1.) room temp., 2.) reflux;

DOI:10.1039/c39860000867

Reference yield: 78.0%

3'-hydroxy-2-methylbenzanilide (55814-53-4) + 1,3-Bis(t-butyldimethylsiloxy)prop-2-yl 2,5-dichlorobenzenesulphonate (105376-71-4) → N-{4-[2-(tert-Butyl-dimethyl-silanyloxy)-1-(tert-butyl-dimethyl-silanyloxymethyl)-ethoxy]-phenyl}-2-methyl-benzamide

Guidance literature:

With 18-crown-6 ether; sodium hydride; In tetrahydrofuran; 1.) room temp., 2.) reflux;

DOI:10.1039/c39860000867

upstream raw materials:

tert-butyldimethylsilyl chloride

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