(3-Ethynylphenyl)methanol

Base Information

Chemical Name:(3-Ethynylphenyl)methanol
CAS No.:10602-07-0
Molecular Formula:C9H8O
Molecular Weight:132.162
Hs Code.:
European Community (EC) Number:838-974-1
DSSTox Substance ID:DTXSID801313408
Nikkaji Number:J1.404.455H

Synonyms:(3-Ethynylphenyl)methanol;10602-07-0;MFCD20527755;3-Ethynylbenzyl alcohol;m-ethynylbenzyl alcohol;3-Ethynylbenzenemethanol;(3-ethynyl-phenyl)-methanol;SCHEMBL510419;ZZIJUXAKPUSHFS-UHFFFAOYSA-N;DTXSID801313408;SY033715;CS-0378923;E85852;EN300-1833515;A922147

Suppliers and Price of (3-Ethynylphenyl)methanol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 9 raw suppliers

Chemical Property of (3-Ethynylphenyl)methanol

Chemical Property:

XLogP3:1.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:132.057514874
Heavy Atom Count:10
Complexity:142

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C#CC1=CC=CC(=C1)CO

Technology Process of (3-Ethynylphenyl)methanol

There total 9 articles about (3-Ethynylphenyl)methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1007587-63-4
3-(trimethylsilyleth-1-yn-1-yl)benzyl alcohol

: 10602-07-0
3-(hydroxymethyl)ethynylbenzene

Guidance literature:: With potassium carbonate; In methanol; at 20 ℃; for 1h;
DOI:10.1021/acs.jmedchem.0c01491

Reference yield: 74.0%

: 208943-28-6
4-[3-(hydroxymethyl)phenyl]-2-methylbut-3-yn-2-ol

: 10602-07-0
3-(hydroxymethyl)ethynylbenzene

Guidance literature:: With potassium hydroxide; In benzene; Heating;
DOI:10.1023/A:1015026200647

Reference yield:

: 15852-73-0
(3-Bromophenyl)methanol

: 10602-07-0
3-(hydroxymethyl)ethynylbenzene

Guidance literature:: Multi-step reaction with 2 steps

1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / 24 h / 20 - 70 °C / Inert atmosphere

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 1.5 h / 20 °C

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tetrabutyl ammonium fluoride; triethylamine; In tetrahydrofuran;
DOI:10.1039/c1cc10582e