Plumbane, methylidynetris[triphenyl-

Base Information

Chemical Name:Plumbane, methylidynetris[triphenyl-
CAS No.:1066-07-5
Molecular Formula:C55H46Pb3
Molecular Weight:1328.57
Hs Code.:

Synonyms:

Suppliers and Price of Plumbane, methylidynetris[triphenyl-

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Plumbane, methylidynetris[triphenyl-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Plumbane, methylidynetris[triphenyl-

There total 2 articles about Plumbane, methylidynetris[triphenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1153-06-6
triphenyllead(IV) chloride

: 1066-07-5
tris(triphenylplumbyl)methane

Guidance literature:: With water; lithium; In tetrahydrofuran; addn. of Li to Ph3PbCl in THF (N2, temp. between room temp. and 40°C, 4 h), excess Li separated, mixt. cooled to -60°C, addn. of CHCl3, warmed to room temp. (30 min), stirred (4 h), addn. of ice-water; extn. with CHCl3, org. layers washed with water, dried (Na2SO4), evapn., crystn. from acetone/ ethanol by slow evapn. of the acetone;

Reference yield: 45.0%

: 76002-47-6
bis(triphenylplumbyl)methyllithium

: 595-89-1
Tetraphenyllead

: 1064-41-1
bis(triphenylplumbyl)methane

: 1066-07-5
tris(triphenylplumbyl)methane

Guidance literature:: With water; In tetrahydrofuran; addn. of Ph4Pb to soln. of (Ph3Pb)2CHLi in THF (N2, -60°C), allowed to warm to 0°C (30 min), stirred (30 min), addn. of water; extn. with CHCl3, org. layers washed with water, dried (Na2SO4), evapn., chromy. (Al2O3, benzine/ benzine-ether; 1. fraction: (Ph3Pb)2CH2, 2. fraction: (Ph3Pb)3CH);

Reference yield: 97.0%

: 1066-07-5
tris(triphenylplumbyl)methane

: 591-51-5
phenyllithium

: 76002-47-6
bis(triphenylplumbyl)methyllithium

Guidance literature:: In tetrahydrofuran; byproducts: tetraphenylplumbane; addn. of 2 molequiv PhLi to (Ph3Pb)3CH in THF (N2, -60°C), warmed to 0°C (pptn. of Ph4Pb); not isolated;