Benzenamine, 2-[(1H-benzimidazol-2-ylsulfinyl)methyl]-4-fluoro-

Base Information

Chemical Name:Benzenamine, 2-[(1H-benzimidazol-2-ylsulfinyl)methyl]-4-fluoro-
CAS No.:106747-38-0
Molecular Formula:C₁₄H₁₂FN₃OS
Molecular Weight:289.333
Hs Code.:

Synonyms:

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Chemical Property of Benzenamine, 2-[(1H-benzimidazol-2-ylsulfinyl)methyl]-4-fluoro-

Chemical Property:

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Safty Information:

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MSDS Files:: SDS file from LookChem

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Technology Process of Benzenamine, 2-[(1H-benzimidazol-2-ylsulfinyl)methyl]-4-fluoro-

There total 6 articles about Benzenamine, 2-[(1H-benzimidazol-2-ylsulfinyl)methyl]-4-fluoro- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 106747-04-0
N-<2-(2-benzimidazolylsulfinyl)methyl>-4-fluorophenylphthalimide

: 106747-38-0
2-<(2-benzimidazolylsulfinyl)methyl>-4-fluoroaniline

Guidance literature:: With hydrazine hydrate; In ethanol; for 3h; Yield given; Ambient temperature;
DOI:10.1021/jm00401a024

Reference yield:

: 452-71-1
4-fluor-2-methylaniline

: 106747-38-0
2-<(2-benzimidazolylsulfinyl)methyl>-4-fluoroaniline

Guidance literature:: Multi-step reaction with 5 steps

1: 1.96 g / 0.5 h / 160 °C

2: N-bromosuccinimide, benzoyl peroxide / 1 h / Irradiation

3: 190 mg / propan-2-ol / 1.5 h / Heating

4: 119 mg / 85percent m-CPBA / CH₂Cl₂ / 0.33 h / -5 °C

5: NH₂NH₂*H₂O / ethanol / 3 h / Ambient temperature

With N-Bromosuccinimide; Perbenzoic acid; hydrazine hydrate; 3-chloro-benzenecarboperoxoic acid; In ethanol; dichloromethane; isopropyl alcohol;
DOI:10.1021/jm00401a024

Reference yield:

: 106747-02-8
N-(4-fluoro-2-methylphenyl)phthalimide

: 106747-38-0
2-<(2-benzimidazolylsulfinyl)methyl>-4-fluoroaniline

Guidance literature:: Multi-step reaction with 4 steps

1: N-bromosuccinimide, benzoyl peroxide / 1 h / Irradiation

2: 190 mg / propan-2-ol / 1.5 h / Heating

3: 119 mg / 85percent m-CPBA / CH₂Cl₂ / 0.33 h / -5 °C

4: NH₂NH₂*H₂O / ethanol / 3 h / Ambient temperature

With N-Bromosuccinimide; Perbenzoic acid; hydrazine hydrate; 3-chloro-benzenecarboperoxoic acid; In ethanol; dichloromethane; isopropyl alcohol;
DOI:10.1021/jm00401a024