2-Piperidinone, 1-methyl-6-[2-[2-(methylsulfonyl)-10H-phenothiazin-10-yl]ethyl]-, S-oxide

Base Information

Chemical Name:2-Piperidinone, 1-methyl-6-[2-[2-(methylsulfonyl)-10H-phenothiazin-10-yl]ethyl]-, S-oxide
CAS No.:106939-04-2
Molecular Formula:C21H24N2O4S2
Molecular Weight:
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Piperidinone, 1-methyl-6-[2-[2-(methylsulfonyl)-10H-phenothiazin-10-yl]ethyl]-, S-oxide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-Piperidinone, 1-methyl-6-[2-[2-(methylsulfonyl)-10H-phenothiazin-10-yl]ethyl]-, S-oxide

There total 7 articles about 2-Piperidinone, 1-methyl-6-[2-[2-(methylsulfonyl)-10H-phenothiazin-10-yl]ethyl]-, S-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 142154-41-4
10-<2-(1-methylpiperidin-2-on-6-yl)ethyl>-2-methylsulfonyl-10H-phenothiazine

: 106939-04-2
10-<2-(1-methylpiperidin-2-on-6-yl)ethyl>-2-methylsulfonyl-10H-phenothiazine-5-sulfoxide

Guidance literature:: With dihydrogen peroxide; In methanol; acetone; for 36h; Ambient temperature;
DOI:10.1002/jhet.5570280202

Reference yield:

: 1484-84-0
2(RS)-(2-hydroxyethyl)piperidine

: 106939-04-2
10-<2-(1-methylpiperidin-2-on-6-yl)ethyl>-2-methylsulfonyl-10H-phenothiazine-5-sulfoxide

Guidance literature:: Multi-step reaction with 7 steps

1: 93 percent / thionyl chloride / CHCl₃ / 2 h / Heating

2: 93 percent / pyridine / 1 h / Ambient temperature

3: 78 percent / 10percent aqueous sodium metaperiodate / ruthenium(IV) oxide / ethyl acetate / 4 h / Ambient temperature

4: 66 percent / basic aluminum oxide / hexane; ethyl acetate / Ambient temperature

5: 87 percent / sodium hydride / dimethylformamide / Ambient temperature

6: 72 percent / sodium hydride / toluene / 22 h / Heating

7: 82 percent / 30percent aqueous hydrogen peroxide / methanol; acetone / 36 h / Ambient temperature

With pyridine; aluminum oxide; sodium periodate; thionyl chloride; dihydrogen peroxide; sodium hydride; ruthenium(IV) oxide; In methanol; hexane; chloroform; ethyl acetate; N,N-dimethyl-formamide; acetone; toluene;
DOI:10.1002/jhet.5570280202

Reference yield:

: 60012-49-9
2-(2-Chloroethyl)piperidine Hydrochloride

: 106939-04-2
10-<2-(1-methylpiperidin-2-on-6-yl)ethyl>-2-methylsulfonyl-10H-phenothiazine-5-sulfoxide

Guidance literature:: Multi-step reaction with 6 steps

1: 93 percent / pyridine / 1 h / Ambient temperature

2: 78 percent / 10percent aqueous sodium metaperiodate / ruthenium(IV) oxide / ethyl acetate / 4 h / Ambient temperature

3: 66 percent / basic aluminum oxide / hexane; ethyl acetate / Ambient temperature

4: 87 percent / sodium hydride / dimethylformamide / Ambient temperature

5: 72 percent / sodium hydride / toluene / 22 h / Heating

6: 82 percent / 30percent aqueous hydrogen peroxide / methanol; acetone / 36 h / Ambient temperature

With pyridine; aluminum oxide; sodium periodate; dihydrogen peroxide; sodium hydride; ruthenium(IV) oxide; In methanol; hexane; ethyl acetate; N,N-dimethyl-formamide; acetone; toluene;
DOI:10.1002/jhet.5570280202