Phosphinecarbothioamide, 1,1-diphenyl-N-(1-phenylethyl)-, (S)-

Base Information

Chemical Name:Phosphinecarbothioamide, 1,1-diphenyl-N-(1-phenylethyl)-, (S)-
CAS No.:107735-11-5
Molecular Formula:C21H20NPS
Molecular Weight:349.436
Hs Code.:
Mol file:107735-11-5.mol

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Phosphinecarbothioamide, 1,1-diphenyl-N-(1-phenylethyl)-, (S)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
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MSDS Files:: SDS file from LookChem

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Technology Process of Phosphinecarbothioamide, 1,1-diphenyl-N-(1-phenylethyl)-, (S)-

There total 2 articles about Phosphinecarbothioamide, 1,1-diphenyl-N-(1-phenylethyl)-, (S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 24277-43-8
(S)-1-phenylethyl isothiocyanate

: 829-85-6
diphenylphosphane

: 107735-11-5
(-)-S-<1-(Diphenylphosphino)-N-(1'-phenylethyl)thioformamid>

Guidance literature:: at 35 - 40 ℃; for 10h;

Reference yield:

: 2627-86-3
(S)-1-phenyl-ethylamine

: 107735-11-5
(-)-S-<1-(Diphenylphosphino)-N-(1'-phenylethyl)thioformamid>

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / DCC / diethyl ether / 5 h / Ambient temperature

2: 100 percent / 10 h / 35 - 40 °C

With dicyclohexyl-carbodiimide; In diethyl ether;

Reference yield: 95.0%

: tricarbonylcyclopentadienyltungsten(II) chloride

: 107735-11-5
(-)-S-<1-(Diphenylphosphino)-N-(1'-phenylethyl)thioformamid>

: (C₅H₅)W(CO)2((C₆H₅)2PCSNCH(C₆H₅)(CH₃))

Guidance literature:: With K₂CO₃ or KOH; In methanol; treatment of (-)-(C6H5)2PCSNHCH(CH3)C6H5 and K2CO3 or KOH in methanol with (C5H5)W(CO)3Cl at room temp.; stirring for 8-10 h;; the ppt. was sucked off, washed with water, and dried in vac.; recrystn. from diethylether; elem. anal.;;