Myrigalon B

Base Information

• Chemical Name: Myrigalon B
• CAS No.: 34328-55-7
• Molecular Formula: C₁₈H₂₀O₄
• Molecular Weight: 300.354
• DSSTox Substance ID: DTXSID101317980
• Metabolomics Workbench ID: 26965
• Nikkaji Number: J742.690I
• Wikidata: Q105252591
• Mol file: 34328-55-7.mol

Synonyms:2',6'-dihydroxy-4'-methoxy-3',5'-dimethyldihydrochalcone;myrigalone B

Chemical Property of Myrigalon B

Chemical Property:

• XLogP3: 4
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 5
• Exact Mass: 300.13615911
• Heavy Atom Count: 22
• Complexity: 348

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=C(C(=C(C(=C1OC)C)O)C(=O)CCC2=CC=CC=C2)O

Technology Process of Myrigalon B

There total 4 articles about Myrigalon B which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-hydroxy-7-methoxy-6,8-dimethylflananone (51621-52-4) → 2',6'-dihydroxy-4'-methoxy-3',5'-dimethyldihydrochalcone (34328-55-7)

Guidance literature:

With potassium hydroxide; hydrogen; palladium on activated charcoal; In methanol;

DOI:10.1016/S0031-9422(00)88753-1

Reference yield:

2,4-dimethylbenzene-1,3,5-triol (4463-02-9) → 2',6'-dihydroxy-4'-methoxy-3',5'-dimethyldihydrochalcone (34328-55-7)

Guidance literature:

Multi-step reaction with 2 steps

1: (i) AlCl₃, CS₂, PhNO₂, (ii) /BRN= 742586/

2: KHCO₃ / diethyl ether; toluene

With potassium hydrogencarbonate; In diethyl ether; toluene;

DOI:10.1016/S0031-9422(00)88754-3

Reference yield:

hydrocinnamic acid chloride (645-45-4) → 2',6'-dihydroxy-4'-methoxy-3',5'-dimethyldihydrochalcone (34328-55-7)

Guidance literature:

Multi-step reaction with 2 steps

1: (i) AlCl₃, CS₂, PhNO₂, (ii) /BRN= 742586/

2: KHCO₃ / diethyl ether; toluene

With potassium hydrogencarbonate; In diethyl ether; toluene;

DOI:10.1016/S0031-9422(00)88754-3

upstream raw materials:

5-hydroxy-7-methoxy-6,8-dimethylflananone

2',4',6'-trihydroxy-3',5'-dimethyldihydrochalcone

dimethyl sulfate

2,4-dimethylbenzene-1,3,5-triol