2(1H)-Quinolinone, 4-azido-3-phenyl-

Base Information

Chemical Name:2(1H)-Quinolinone, 4-azido-3-phenyl-
CAS No.:108832-08-2
Molecular Formula:C15H10N4O
Molecular Weight:262.271
Hs Code.:
DSSTox Substance ID:DTXSID00382939
Wikidata:Q82174428

Synonyms:2(1H)-Quinolinone, 4-azido-3-phenyl-;108832-08-2;DTXSID00382939;4-Azido-3-phenyl-2(1 H)-chinolon

Suppliers and Price of 2(1H)-Quinolinone, 4-azido-3-phenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 2(1H)-Quinolinone, 4-azido-3-phenyl-

Chemical Property:

XLogP3:3.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:262.08546096
Heavy Atom Count:20
Complexity:472

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C2=C(C3=CC=CC=C3NC2=O)N=[N+]=[N-]

Technology Process of 2(1H)-Quinolinone, 4-azido-3-phenyl-

There total 2 articles about 2(1H)-Quinolinone, 4-azido-3-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.7%

: 108832-06-0
3-Phenyl-4-tosyloxy-2(1H)-chinolon

: 108832-08-2
4-Azido-3-phenyl-2(1H)-chinolon

Guidance literature:: With sodium azide; In N,N-dimethyl-formamide; at 20 ℃; for 2h;
DOI:10.1007/BF00810876

Reference yield:

: 14933-29-0
4-hydroxy-3-phenyl-2(1H)-quinolone

: 108832-08-2
4-Azido-3-phenyl-2(1H)-chinolon

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / p-(N,N-dimethylamino)-pyridine / pyridine / 2 h / Ambient temperature

2: 59.7 percent / NaN₃ / dimethylformamide / 2 h / 20 °C

With sodium azide; dmap; In pyridine; N,N-dimethyl-formamide;
DOI:10.1007/BF00810876