Benzoic acid, 3,4-dihydroxy-5-methoxy-, butyl ester

Base Information

Chemical Name:Benzoic acid, 3,4-dihydroxy-5-methoxy-, butyl ester
CAS No.:108853-29-8
Molecular Formula:C12H16O5
Molecular Weight:240.256
Hs Code.:
Mol file:108853-29-8.mol

Synonyms:

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Chemical Property of Benzoic acid, 3,4-dihydroxy-5-methoxy-, butyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
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MSDS Files:: SDS file from LookChem

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Technology Process of Benzoic acid, 3,4-dihydroxy-5-methoxy-, butyl ester

There total 1 articles about Benzoic acid, 3,4-dihydroxy-5-methoxy-, butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1083-41-6
n-butyl gallate

: 77-78-1
dimethyl sulfate

: 108853-29-8
n-butyl 3,4-dihydroxy-5-methoxybenzoate

Guidance literature:: With sodium hydroxide; boric acid; Ambient temperature;
DOI:10.1016/S0031-9422(00)82361-4

Reference yield:

: 108853-29-8
n-butyl 3,4-dihydroxy-5-methoxybenzoate

: 5780-07-4
3-methoxy-4,5-methylenedioxybenzaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: 1.90 g / K₂CO₃, CuO / dimethylformamide / 3 h / 120 - 125 °C

2: 980 mg / LiAlH₄ / tetrahydrofuran / 2 h / Ambient temperature

3: 140 mg / pyridiniumchlorochromate / CH₂Cl₂

With lithium aluminium tetrahydride; potassium carbonate; pyridinium chlorochromate; copper(II) oxide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0031-9422(00)82361-4

Reference yield:

: 108853-29-8
n-butyl 3,4-dihydroxy-5-methoxybenzoate

: 3,3′-dimethoxy-4,5-methylenedioxybibenzyl

Guidance literature:: Multi-step reaction with 6 steps

1: 1.90 g / K₂CO₃, CuO / dimethylformamide / 3 h / 120 - 125 °C

2: 980 mg / LiAlH₄ / tetrahydrofuran / 2 h / Ambient temperature

3: 850 mg / 47percent HBr / benzene / 2 h / Ambient temperature

4: 1.53 g / dimethylformamide / 3 h / Heating

5: NaOEt / ethanol

6: H₂ / PtO₂ / acetic acid

With lithium aluminium tetrahydride; hydrogen bromide; hydrogen; sodium ethanolate; potassium carbonate; copper(II) oxide; platinum(IV) oxide; In tetrahydrofuran; ethanol; acetic acid; N,N-dimethyl-formamide; benzene;
DOI:10.1016/S0031-9422(00)82361-4