2-(4-Bromo-2-methoxyphenyl)-1,3-dioxolane

Base Information

Chemical Name:2-(4-Bromo-2-methoxyphenyl)-1,3-dioxolane
CAS No.:109142-86-1
Molecular Formula:C10H11BrO3
Molecular Weight:259.1
Hs Code.:
DSSTox Substance ID:DTXSID20546632
Wikidata:Q82424522
Mol file:109142-86-1.mol

Synonyms:109142-86-1;2-(4-Bromo-2-methoxyphenyl)-1,3-dioxolane;2-(4-Bromo-2-methoxyphenyl)-[1,3]dioxolane;1,3-Dioxolane, 2-(4-bromo-2-methoxyphenyl)-;SCHEMBL1704526;DTXSID20546632;MFCD28368830;CS-0193378;E93506

Suppliers and Price of 2-(4-Bromo-2-methoxyphenyl)-1,3-dioxolane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

AOBChem
2-(4-Bromo-2-methoxyphenyl)-[1,3]dioxolane 95%
100g
$ 2369.00

Total 6 raw suppliers

Chemical Property of 2-(4-Bromo-2-methoxyphenyl)-1,3-dioxolane

Chemical Property:

PSA：27.69000
LogP:2.50310
XLogP3:2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:257.98916
Heavy Atom Count:14
Complexity:182

Purity/Quality:

97% ^*data from raw suppliers

2-(4-Bromo-2-methoxyphenyl)-[1,3]dioxolane 95% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=C(C=CC(=C1)Br)C2OCCO2

Technology Process of 2-(4-Bromo-2-methoxyphenyl)-1,3-dioxolane

There total 3 articles about 2-(4-Bromo-2-methoxyphenyl)-1,3-dioxolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 43192-33-2
4-bromo-2-methoxybenzaldehyde

: 107-21-1
ethylene glycol

: 109142-86-1
(bromo-4 methoxy-2 phenyl)-2 dioxolanne-1,3

Guidance literature:: With toluene-4-sulfonic acid; In toluene; for 3h; Heating; Dean-Stark apparate;

Reference yield:

: 2398-37-0
3-methoxyphenyl bromide

: 109142-86-1
(bromo-4 methoxy-2 phenyl)-2 dioxolanne-1,3

Guidance literature:: Multi-step reaction with 3 steps

1: 1) TiCl₄ 2) AcCl₃ / 2) CH₂Cl₂, 20 deg C, 4 h

2: 100 percent / K₂CO₃ / acetone / 0.75 h / Heating

3: 91 percent / p-toluenesulfonic acid / toluene / 3 h / Heating; Dean-Stark apparate

With titanium tetrachloride; potassium carbonate; toluene-4-sulfonic acid; In acetone; toluene;

Reference yield:

: 57848-46-1
4-bromo-2-fluorobenzaldehyde

: 109142-86-1
(bromo-4 methoxy-2 phenyl)-2 dioxolanne-1,3

Guidance literature:: Multi-step reaction with 2 steps

1: methanol / 1 h / 0 - 70 °C

2: toluene-4-sulfonic acid / toluene / 2 h / 110 - 115 °C / Dean-Stark

With toluene-4-sulfonic acid; In methanol; toluene;