Carbamic acid, [1-[[4-(phenylmethoxy)phenyl]methyl]-5-[(tetrahydro-2H-pyran-2-yl)oxy]-2 -pentenyl]-, 1,1-dimethylethyl ester, (E)-

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Chemical Name:Carbamic acid, [1-[[4-(phenylmethoxy)phenyl]methyl]-5-[(tetrahydro-2H-pyran-2-yl)oxy]-2 -pentenyl]-, 1,1-dimethylethyl ester, (E)-
CAS No.:109687-62-9
Molecular Formula:C29H39NO5
Molecular Weight:481.632
Hs Code.:
Mol file:109687-62-9.mol

Synonyms:

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Chemical Property of Carbamic acid, [1-[[4-(phenylmethoxy)phenyl]methyl]-5-[(tetrahydro-2H-pyran-2-yl)oxy]-2 -pentenyl]-, 1,1-dimethylethyl ester, (E)-

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Technology Process of Carbamic acid, [1-[[4-(phenylmethoxy)phenyl]methyl]-5-[(tetrahydro-2H-pyran-2-yl)oxy]-2 -pentenyl]-, 1,1-dimethylethyl ester, (E)-

There total 4 articles about Carbamic acid, [1-[[4-(phenylmethoxy)phenyl]methyl]-5-[(tetrahydro-2H-pyran-2-yl)oxy]-2 -pentenyl]-, 1,1-dimethylethyl ester, (E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 4248-19-5
tert-butyl carbazate

: 109687-61-8
4-(phenylseleno)-1-<4-(phenylmethoxy)phenyl>-6-<(2-tetrahydropyranyl)oxy>-trans-2-hexene

: 109687-62-9
2-<(tert-butoxycarbonyl)amino>-1-<4-(phenylmethoxy)-phenyl>-6-<(2-tetrahydropyranyl)oxy>-trans-3-hexene

Guidance literature:: With N-chloro-succinimide; triethylamine;
DOI:10.1021/jo00226a007

Reference yield:

: 5544-60-5
4-(benzyloxy)benzyl bromide

: 109687-62-9
2-<(tert-butoxycarbonyl)amino>-1-<4-(phenylmethoxy)-phenyl>-6-<(2-tetrahydropyranyl)oxy>-trans-3-hexene

Guidance literature:: Multi-step reaction with 4 steps

1: 1.)LDA / 1.) hexane, THF, -78 deg C, 0.5 h, 2) hexane, THF, -78 deg C, 2h

2: 92 percent / p-toluenesulfonic acid / benzene / 3 h / Heating

3: LDA / 1.) hexane, THF, -78 deg C, 0.5 h, 2.) hexane, THF, -78 deg C, 2 h

4: 57 percent / N-chlorosuccinimide, triethylamine

With N-chloro-succinimide; toluene-4-sulfonic acid; triethylamine; lithium diisopropyl amide; In benzene;
DOI:10.1021/jo00226a007

Reference yield:

: 109687-59-4
3-(phenylseleno)-4-<(4-phenylmethoxy)phenyl>butene

: 109687-62-9
2-<(tert-butoxycarbonyl)amino>-1-<4-(phenylmethoxy)-phenyl>-6-<(2-tetrahydropyranyl)oxy>-trans-3-hexene

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / p-toluenesulfonic acid / benzene / 3 h / Heating

2: LDA / 1.) hexane, THF, -78 deg C, 0.5 h, 2.) hexane, THF, -78 deg C, 2 h

3: 57 percent / N-chlorosuccinimide, triethylamine

With N-chloro-succinimide; toluene-4-sulfonic acid; triethylamine; lithium diisopropyl amide; In benzene;
DOI:10.1021/jo00226a007