1-Bromo-2,3-dichloro-4-methoxybenzene

Base Information

Chemical Name:1-Bromo-2,3-dichloro-4-methoxybenzene
CAS No.:109803-52-3
Molecular Formula:C7H5BrCl2O
Molecular Weight:255.926
Hs Code.:
DSSTox Substance ID:DTXSID301335001
Nikkaji Number:J1.617.534J
Mol file:109803-52-3.mol

Synonyms:1-Bromo-2,3-dichloro-4-methoxybenzene;109803-52-3;bromodichloroanisole;SCHEMBL6865460;BTRCDLZQISXWHZ-UHFFFAOYSA-N;DTXSID301335001;MFCD21609662;4-Bromo-2,3-dichloro-1-methoxybenzene;CS-0211090;G62846

Suppliers and Price of 1-Bromo-2,3-dichloro-4-methoxybenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 1-Bromo-2,3-dichloro-4-methoxybenzene

Chemical Property:

XLogP3:3.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:253.89008
Heavy Atom Count:11
Complexity:134

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COC1=C(C(=C(C=C1)Br)Cl)Cl

Technology Process of 1-Bromo-2,3-dichloro-4-methoxybenzene

There total 4 articles about 1-Bromo-2,3-dichloro-4-methoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1940-44-9
4-bromo-2,3-dichlorophenol

: 74-88-4
methyl iodide

: 109803-52-3
1-bromo-2,3-dichloro-4-methoxybenzene

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 70 ℃; for 3h;

Reference yield: 66.0%

: 1984-59-4
2,3-dichloroanisole

: 109803-52-3
1-bromo-2,3-dichloro-4-methoxybenzene

Guidance literature:: With bromine; iron; at 90 ℃; for 4h;
DOI:10.1021/jm00393a020

Reference yield:

: 576-24-9
2,3-dichlorophenol

: 109803-52-3
1-bromo-2,3-dichloro-4-methoxybenzene

Guidance literature:: Multi-step reaction with 2 steps

1: 53 percent / bromine / CH₂Cl₂ / 2 h

2: 77 percent / Cs₂CO₃ / dimethylformamide / 3 h / 70 °C

With bromine; caesium carbonate; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm049967u