2-Cyclohexene-1-methanol, 4-[3-(3,3-dimethyloxiranyl)-1-methylpropyl]-6-[4-[(tetrahydro-2H-pyran-2- yl)oxy]-1-butenyl]-5-[[(tetrahydro-2H-pyran-2-yl)oxy]methyl]-, acetate

Base Information

Chemical Name:2-Cyclohexene-1-methanol, 4-[3-(3,3-dimethyloxiranyl)-1-methylpropyl]-6-[4-[(tetrahydro-2H-pyran-2- yl)oxy]-1-butenyl]-5-[[(tetrahydro-2H-pyran-2-yl)oxy]methyl]-, acetate
CAS No.:110188-96-0
Molecular Formula:C₃₂H₅₂O₇
Molecular Weight:548.761
Hs Code.:

2-Cyclohexene-1-methanol,
4-[3-(3,3-dimethyloxiranyl)-1-methylpropyl]-6-[4-[(tetrahydro-2H-pyran-2-
yl)oxy]-1-butenyl]-5-[[(tetrahydro-2H-pyran-2-yl)oxy]methyl]-, acetate

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Chemical Property of 2-Cyclohexene-1-methanol, 4-[3-(3,3-dimethyloxiranyl)-1-methylpropyl]-6-[4-[(tetrahydro-2H-pyran-2- yl)oxy]-1-butenyl]-5-[[(tetrahydro-2H-pyran-2-yl)oxy]methyl]-, acetate

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Technology Process of 2-Cyclohexene-1-methanol, 4-[3-(3,3-dimethyloxiranyl)-1-methylpropyl]-6-[4-[(tetrahydro-2H-pyran-2- yl)oxy]-1-butenyl]-5-[[(tetrahydro-2H-pyran-2-yl)oxy]methyl]-, acetate

There total 1 articles about 2-Cyclohexene-1-methanol, 4-[3-(3,3-dimethyloxiranyl)-1-methylpropyl]-6-[4-[(tetrahydro-2H-pyran-2- yl)oxy]-1-butenyl]-5-[[(tetrahydro-2H-pyran-2-yl)oxy]methyl]-, acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108-24-7
acetic anhydride

: 110188-95-9,110222-77-0
[(1R,4S,5R,6R)-4-((S)-1,5-Dimethyl-hex-4-enyl)-6-[(Z)-4-(tetrahydro-pyran-2-yloxy)-but-1-enyl]-5-(tetrahydro-pyran-2-yloxymethyl)-cyclohex-2-enyl]-methanol

: 110188-96-0
Acetic acid (1R,4S,5R,6R)-4-[(S)-3-(3,3-dimethyl-oxiranyl)-1-methyl-propyl]-6-[(Z)-4-(tetrahydro-pyran-2-yloxy)-but-1-enyl]-5-(tetrahydro-pyran-2-yloxymethyl)-cyclohex-2-enylmethyl ester

Guidance literature:: With dmap; triethylamine; 3-chloro-benzenecarboperoxoic acid; Yield given. Multistep reaction; 1.) CH₂Cl₂, 1h; 2.) CH₂Cl₂, 0 deg C;
DOI:10.1016/S0040-4039(00)85070-4

Reference yield:

: 110188-96-0
Acetic acid (1R,4S,5R,6R)-4-[(S)-3-(3,3-dimethyl-oxiranyl)-1-methyl-propyl]-6-[(Z)-4-(tetrahydro-pyran-2-yloxy)-but-1-enyl]-5-(tetrahydro-pyran-2-yloxymethyl)-cyclohex-2-enylmethyl ester

: 110188-97-1
[(1R,2R,3R,4R)-4-((S)-1,5-Dimethyl-hex-4-enyl)-2-[4-(tetrahydro-pyran-2-yloxy)-butyl]-3-(tetrahydro-pyran-2-yloxymethyl)-cyclohexyl]-methanol

Guidance literature:: With hydrogen; potassium selenocyanate; Rh/Al₂O₃; Yield given. Multistep reaction; 1.) MeOH, 30 min; 2.) MeOH-H₂O(9:1), 65 deg C, 4d;
DOI:10.1016/S0040-4039(00)85070-4

Reference yield:

: 110188-96-0
Acetic acid (1R,4S,5R,6R)-4-[(S)-3-(3,3-dimethyl-oxiranyl)-1-methyl-propyl]-6-[(Z)-4-(tetrahydro-pyran-2-yloxy)-but-1-enyl]-5-(tetrahydro-pyran-2-yloxymethyl)-cyclohex-2-enylmethyl ester

: 110188-99-3
(1R,2S,6R)-6-((S)-1,5-Dimethyl-hex-4-enyl)-3-methylene-2-(4-oxo-butyl)-cyclohexanecarbaldehyde

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) H₂(50 psi); 2.) KSeCN / 1.) 5percent Rh/Al₂O₃ / 1.) MeOH, 30 min; 2.) MeOH-H₂O(9:1), 65 deg C, 4d

2: 1.) o-nitrophenylselenocyanate-tributylphosphine; 2.) 30percent H₂O₂ / 1.) THF, 2h; 2.) THF, 1h

3: EtOH / PPTS / 10 h / 55 °C

4: 1.) (COCl)2, DMSO; 2.) i-Pr₂NEt / 1.) CH₂Cl₂, -78 deg C, 1h; -78 deg C, 30 min, then room temp., 30 min

With ortho-nitrophenyl selenocyanate; oxalyl dichloride; ethanol; tributylphosphine; hydrogen; dihydrogen peroxide; potassium selenocyanate; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine; Rh/Al₂O₃; pyridinium p-toluenesulfonate;
DOI:10.1016/S0040-4039(00)85070-4