Benzoic acid, 2-hydroxy-6-(10-pentadecenyl)-, (Z)-

Base Information

Chemical Name:Benzoic acid, 2-hydroxy-6-(10-pentadecenyl)-, (Z)-
CAS No.:110202-77-2
Molecular Formula:C22H34O3
Molecular Weight:346.51
Hs Code.:
Mol file:110202-77-2.mol

Synonyms:

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Chemical Property of Benzoic acid, 2-hydroxy-6-(10-pentadecenyl)-, (Z)-

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Technology Process of Benzoic acid, 2-hydroxy-6-(10-pentadecenyl)-, (Z)-

There total 18 articles about Benzoic acid, 2-hydroxy-6-(10-pentadecenyl)-, (Z)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 114802-15-2
2-Methoxy-6-<(Z)-10-pentadecenyl>benzoic acid

: 110202-77-2
(Z)-2-hydroxy-6-(pentadec-10-en-1-yl)-benzoic acid

Guidance literature:: With sodium hydride; ethanethiol; In N,N-dimethyl-formamide; 1.) 0 deg C 15 min; 2.) 140 deg C 3 h;
DOI:10.1016/S0040-4020(01)81629-X

Reference yield:

: 2774-84-7
undec-10-yn-1-ol

: 110202-77-2
(Z)-2-hydroxy-6-(pentadec-10-en-1-yl)-benzoic acid

Guidance literature:: Multi-step reaction with 10 steps

1: p-TsOH*H₂O / 2 h / Ambient temperature

2: n-BuLi / tetrahydrofuran; hexane

3: p-TsOH*H₂O / methanol / 1 h / Heating

4: 100 percent / pyridine / 3.5 h / Ambient temperature

5: 62 percent / dichloromaleic anhydride / 200 °C

6: 94 percent / 2 M KOH / ethanol / Heating

7: 68 percent / CBr₄, PPh₃ / CH₂Cl₂ / Ambient temperature

8: 63 percent / n-BuLi / tetrahydrofuran; hexane; hexamethylphosphoric acid triamide

9: 98 percent / H₂, quinoline / 5percent Pd/CaCO₃ / cyclohexane / 750.06 Torr

10: 86 percent / AlI₃, cyclohexene / CS₂ / Heating

With pyridine; quinoline; potassium hydroxide; aluminium(III) iodide; n-butyllithium; dichloromaleic acid anhydride; carbon tetrabromide; hydrogen; toluene-4-sulfonic acid; triphenylphosphine; cyclohexene; Lindlar's catalyst; In tetrahydrofuran; methanol; carbon disulfide; N,N,N,N,N,N-hexamethylphosphoric triamide; ethanol; hexane; dichloromethane; cyclohexane;

Reference yield:

: 51953-88-9,151329-50-9
1-[(tetrahydropyran-2-yl)oxy]undec-10-yne

: 110202-77-2
(Z)-2-hydroxy-6-(pentadec-10-en-1-yl)-benzoic acid

Guidance literature:: Multi-step reaction with 9 steps

1: n-BuLi / tetrahydrofuran; hexane

2: p-TsOH*H₂O / methanol / 1 h / Heating

3: 100 percent / pyridine / 3.5 h / Ambient temperature

4: 62 percent / dichloromaleic anhydride / 200 °C

5: 94 percent / 2 M KOH / ethanol / Heating

6: 68 percent / CBr₄, PPh₃ / CH₂Cl₂ / Ambient temperature

7: 63 percent / n-BuLi / tetrahydrofuran; hexane; hexamethylphosphoric acid triamide

8: 98 percent / H₂, quinoline / 5percent Pd/CaCO₃ / cyclohexane / 750.06 Torr

9: 86 percent / AlI₃, cyclohexene / CS₂ / Heating

With pyridine; quinoline; potassium hydroxide; aluminium(III) iodide; n-butyllithium; dichloromaleic acid anhydride; carbon tetrabromide; hydrogen; toluene-4-sulfonic acid; triphenylphosphine; cyclohexene; Lindlar's catalyst; In tetrahydrofuran; methanol; carbon disulfide; N,N,N,N,N,N-hexamethylphosphoric triamide; ethanol; hexane; dichloromethane; cyclohexane;