N-dodecyl-2-hydroxybenzamide

Base Information

• Chemical Name: N-dodecyl-2-hydroxybenzamide
• CAS No.: 10586-70-6
• Molecular Formula: C19H31 N O2
• Molecular Weight: 305.4549
• NSC Number: 195348
• DSSTox Substance ID: DTXSID10307855
• Wikidata: Q82055434

Synonyms:10586-70-6;N-dodecyl-2-hydroxybenzamide;N-dodecylsalicylamide;NSC195348;SBB057128;SCHEMBL10697836;DTXSID10307855;AKOS024364867;NSC-195348

Chemical Property of N-dodecyl-2-hydroxybenzamide

Chemical Property:

• Vapor Pressure: 3.79E-09mmHg at 25°C
• Boiling Point: 461.8°Cat760mmHg
• Flash Point: 233.1°C
• Density: 0.986g/cm³
• XLogP3: 6.9
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 12
• Exact Mass: 305.235479232
• Heavy Atom Count: 22
• Complexity: 281

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCCCCCCCCCCCNC(=O)C1=CC=CC=C1O

Technology Process of N-dodecyl-2-hydroxybenzamide

There total 3 articles about N-dodecyl-2-hydroxybenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

n-Dodecylamine (124-22-1) + 2-hydroxy-benzoic acid ethyl ester (118-61-6) → N-dodecyl-2-hydroxybenzamide (10586-70-6)

Guidance literature:

With phenylboronic acid; In neat (no solvent); at 60 ℃; for 0.75h; Reagent/catalyst; Solvent; Microwave irradiation; Green chemistry;

DOI:10.1039/c7ra11434f

Reference yield:

n-Dodecylamine (124-22-1) + phenyl Salicylate (118-55-8) → N-dodecyl-2-hydroxybenzamide (10586-70-6)

Guidance literature:

With 1,2,4-Trichlorobenzene;

DOI:10.1021/ja01203a509

Reference yield:

2-acetoxy-benzoic acid dodecylamide (102377-14-0) → N-dodecyl-2-hydroxybenzamide (10586-70-6)

Guidance literature:

With sodium hydroxide;

DOI:10.1007/BF02884943

upstream raw materials:

2-acetoxy-benzoic acid dodecylamide

n-Dodecylamine

phenyl Salicylate

2-hydroxy-benzoic acid ethyl ester

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