(5,6-Dimethyl-1h-benzimidazol-1-yl)methanol

Base Information

Chemical Name:(5,6-Dimethyl-1h-benzimidazol-1-yl)methanol
CAS No.:19539-34-5
Molecular Formula:C₁₀H₁₂N₂O
Molecular Weight:176.218
Hs Code.:2933990090
European Community (EC) Number:654-677-8
NSC Number:163162
DSSTox Substance ID:DTXSID60941309
Wikidata:Q82918101
Mol file:19539-34-5.mol

Synonyms:19539-34-5;(5,6-dimethyl-1h-benzimidazol-1-yl)methanol;(5,6-dimethylbenzimidazol-1-yl)methanol;1H-Benzimidazole-1-methanol,5,6-dimethyl-;(5,6-dimethyl-1H-1,3-benzodiazol-1-yl)methanol;1H-Benzimidazole-1-methanol,5,6-dimethyl-(9CI);5,6-DIMETHYL-1-BENZIMIDAZOLEMETHANOL;NSC163162;DTXSID60941309;AKOS024332214;NSC-163162;(5,6-Dimethyl-1H-benzo[d]imidazol-1-yl)methanol

Suppliers and Price of (5,6-Dimethyl-1h-benzimidazol-1-yl)methanol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
5,6-Dimethyl-1-benzimidazolemethanol
500mg
$ 350.00

Sigma-Aldrich
5,6-DIMETHYL-1-BENZIMIDAZOLEMETHANOL Aldrich
250mg
$ 144.00

Total 4 raw suppliers

Chemical Property of (5,6-Dimethyl-1h-benzimidazol-1-yl)methanol

Chemical Property:

Vapor Pressure:1.22E-05mmHg at 25°C
Boiling Point:354.6°Cat760mmHg
Flash Point:168.2°C
PSA：38.05000
Density:1.19g/cm³
LogP:1.60290
XLogP3:1.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:176.094963011
Heavy Atom Count:13
Complexity:186

Purity/Quality:

99% ^*data from raw suppliers

5,6-Dimethyl-1-benzimidazolemethanol ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC2=C(C=C1C)N(C=N2)CO

Technology Process of (5,6-Dimethyl-1h-benzimidazol-1-yl)methanol

There total 2 articles about (5,6-Dimethyl-1h-benzimidazol-1-yl)methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.5%

: 582-60-5
5,6-dimethyl-1H-benzo[d]imida-zole

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 19539-34-5
(5,6-dimethyl-benzoimidazol-1-yl)-methanol

Guidance literature:: With methanol; In water; for 3h; Inert atmosphere; Reflux;
DOI:10.1021/om100388w

Reference yield:

: 19539-34-5
(5,6-dimethyl-benzoimidazol-1-yl)-methanol

Guidance literature:: 5,6-Dimethylbenzimidazol, Formalin;

Reference yield:

: 19539-34-5
(5,6-dimethyl-benzoimidazol-1-yl)-methanol

: 1338599-08-8
P(C₆H₁₁)2CH₂N₂HCC₆H₂(CH₃)2

Guidance literature:: Multi-step reaction with 2 steps

1.1: thionyl chloride / dichloromethane / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran / -78 °C / Inert atmosphere

2.2: 12 h / 0 - 20 °C / Inert atmosphere

With n-butyllithium; thionyl chloride; In tetrahydrofuran; dichloromethane;
DOI:10.1021/om200689r