Morpholine, 4-[(3-phenyloxiranyl)sulfonyl]-, cis-

Base Information

Chemical Name:Morpholine, 4-[(3-phenyloxiranyl)sulfonyl]-, cis-
CAS No.:110381-01-6
Molecular Formula:C12H15NO4S
Molecular Weight:269.321
Hs Code.:
Mol file:110381-01-6.mol

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Morpholine, 4-[(3-phenyloxiranyl)sulfonyl]-, cis-

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Technology Process of Morpholine, 4-[(3-phenyloxiranyl)sulfonyl]-, cis-

There total 7 articles about Morpholine, 4-[(3-phenyloxiranyl)sulfonyl]-, cis- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 110381-12-9
4-((Z)-2-Phenyl-ethenesulfonyl)-morpholine

: 110381-01-6
4-((2S,3R)-3-Phenyl-oxiranesulfonyl)-morpholine

Guidance literature:: With potassium hydroxide; potassium hypochlorite; tetra(n-butyl)ammonium hydrogensulfate; In dichloromethane; at 20 ℃; for 14h;
DOI:10.1021/jm00395a010

Reference yield:

: 22457-12-1
4-((bromomethyl)sulfonyl)morpholine

: 110381-01-6
4-((2S,3R)-3-Phenyl-oxiranesulfonyl)-morpholine

Guidance literature:: Multi-step reaction with 5 steps

1: 50percent aq. NaOH, Bu₄N⁽¹⁺⁾*HSO₄^(1-), HMPT

2: Br₂ / CCl₄ / 2.5 h / Heating

3: t-BuOK / dioxane; 2-methyl-propan-2-ol / 3 h / Ambient temperature

4: aq. NaPO₂H₂ / 10percent Pd/C / ethanol / 15 h / Heating

5: 70 percent / KOCl, conc. KOH, tetrabutylammonium hydrogen sulfate / CH₂Cl₂ / 14 h / 20 °C

With N,N,N,N,N,N-hexamethylphosphoric triamide; potassium hydroxide; sodium hydroxide; sodium hypophosphite; potassium hypochlorite; potassium tert-butylate; bromine; tetra(n-butyl)ammonium hydrogensulfate; palladium on activated charcoal; In 1,4-dioxane; tetrachloromethane; ethanol; dichloromethane; tert-butyl alcohol;
DOI:10.1021/jm00395a010

Reference yield:

: 17299-32-0
(E)-4-<(2-phenylethynyl)sulfonyl>morpholine

: 110381-01-6
4-((2S,3R)-3-Phenyl-oxiranesulfonyl)-morpholine

Guidance literature:: Multi-step reaction with 4 steps

1: Br₂ / CCl₄ / 2.5 h / Heating

2: t-BuOK / dioxane; 2-methyl-propan-2-ol / 3 h / Ambient temperature

3: aq. NaPO₂H₂ / 10percent Pd/C / ethanol / 15 h / Heating

4: 70 percent / KOCl, conc. KOH, tetrabutylammonium hydrogen sulfate / CH₂Cl₂ / 14 h / 20 °C

With potassium hydroxide; sodium hypophosphite; potassium hypochlorite; potassium tert-butylate; bromine; tetra(n-butyl)ammonium hydrogensulfate; palladium on activated charcoal; In 1,4-dioxane; tetrachloromethane; ethanol; dichloromethane; tert-butyl alcohol;
DOI:10.1021/jm00395a010