Benzeneacetaldehyde, a-[2-(acetyloxy)ethyl]-2-(methoxymethoxy)-

Base Information

Chemical Name:Benzeneacetaldehyde, a-[2-(acetyloxy)ethyl]-2-(methoxymethoxy)-
CAS No.:110451-77-9
Molecular Formula:C14H18O5
Molecular Weight:266.294
Hs Code.:

Synonyms:

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Chemical Property of Benzeneacetaldehyde, a-[2-(acetyloxy)ethyl]-2-(methoxymethoxy)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of Benzeneacetaldehyde, a-[2-(acetyloxy)ethyl]-2-(methoxymethoxy)-

There total 5 articles about Benzeneacetaldehyde, a-[2-(acetyloxy)ethyl]-2-(methoxymethoxy)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 110451-76-8
Acetic acid 4-hydroxy-3-(2-methoxymethoxy-phenyl)-butyl ester

: 110451-77-9
Acetic acid 3-(2-methoxymethoxy-phenyl)-4-oxo-butyl ester

Guidance literature:: With pyridinium chlorochromate; In dichloromethane; at 20 ℃; for 6h;

Reference yield:

: 110451-69-9
2-(1-Benzyloxymethyl-allyl)-phenol

: 110451-77-9
Acetic acid 3-(2-methoxymethoxy-phenyl)-4-oxo-butyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 92 percent / sodium hydride / dimethylformamide / Ambient temperature

2: 76 percent / 9-borabicyclo<3,3,1>nonane, aq. sodium hydroxide, hydrogen peroxide / ethanol

3: pyridine / 16 h / 20 °C

4: hydrogen / 10percent palladium-carbon / ethanol / 0.33 h / 23 °C

5: 88 percent / pyridinium chlorochromate / CH₂Cl₂ / 6 h / 20 °C

With pyridine; sodium hydroxide; 9-borabicyclo[3.3.1]nonane dimer; hydrogen; dihydrogen peroxide; sodium hydride; pyridinium chlorochromate; palladium on activated charcoal; In ethanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 110451-70-2
1-(1-Benzyloxymethyl-allyl)-2-methoxymethoxy-benzene

: 110451-77-9
Acetic acid 3-(2-methoxymethoxy-phenyl)-4-oxo-butyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 76 percent / 9-borabicyclo<3,3,1>nonane, aq. sodium hydroxide, hydrogen peroxide / ethanol

2: pyridine / 16 h / 20 °C

3: hydrogen / 10percent palladium-carbon / ethanol / 0.33 h / 23 °C

4: 88 percent / pyridinium chlorochromate / CH₂Cl₂ / 6 h / 20 °C

With pyridine; sodium hydroxide; 9-borabicyclo[3.3.1]nonane dimer; hydrogen; dihydrogen peroxide; pyridinium chlorochromate; palladium on activated charcoal; In ethanol; dichloromethane;