4-Benzyloxy-3-(2-methoxymethoxy-phenyl)-butan-1-ol

Base Information

Chemical Name:4-Benzyloxy-3-(2-methoxymethoxy-phenyl)-butan-1-ol
CAS No.:110451-71-3
Molecular Formula:C₁₉H₂₄O₄
Molecular Weight:316.397
Hs Code.:

Synonyms:4-Benzyloxy-3-(2-methoxymethoxy-phenyl)-butan-1-ol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-Benzyloxy-3-(2-methoxymethoxy-phenyl)-butan-1-ol

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of 4-Benzyloxy-3-(2-methoxymethoxy-phenyl)-butan-1-ol

There total 7 articles about 4-Benzyloxy-3-(2-methoxymethoxy-phenyl)-butan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 110451-70-2
1-(1-Benzyloxymethyl-allyl)-2-methoxymethoxy-benzene

: 110451-71-3
4-Benzyloxy-3-(2-methoxymethoxy-phenyl)-butan-1-ol

Guidance literature:: With sodium hydroxide; 9-borabicyclo[3.3.1]nonane dimer; dihydrogen peroxide; In ethanol;

Reference yield:

: 80885-30-9,81028-03-7,69152-88-1
(E)-4-(benzyloxy)-2-buten-1-ol

: 110451-71-3
4-Benzyloxy-3-(2-methoxymethoxy-phenyl)-butan-1-ol

Guidance literature:: Multi-step reaction with 5 steps

1: phosphorus tribromide / diethyl ether / 0 degC, 2 h then allowed to warm to room temperature

2: potassium carbonate / acetone / 16 h / Heating

3: 72 percent / neat (no solvent) / 0.5 h / Heating

4: 92 percent / sodium hydride / dimethylformamide / Ambient temperature

5: 76 percent / 9-borabicyclo<3,3,1>nonane, aq. sodium hydroxide, hydrogen peroxide / ethanol

With sodium hydroxide; 9-borabicyclo[3.3.1]nonane dimer; dihydrogen peroxide; phosphorus tribromide; sodium hydride; potassium carbonate; In diethyl ether; ethanol; N,N-dimethyl-formamide; acetone;

Reference yield:

: 91142-50-6
4-benzyloxy-2-butyn-1-ol

: 110451-71-3
4-Benzyloxy-3-(2-methoxymethoxy-phenyl)-butan-1-ol

Guidance literature:: Multi-step reaction with 6 steps

1: 65 percent / lithium aluminium hydride / tetrahydrofuran

2: phosphorus tribromide / diethyl ether / 0 degC, 2 h then allowed to warm to room temperature

3: potassium carbonate / acetone / 16 h / Heating

4: 72 percent / neat (no solvent) / 0.5 h / Heating

5: 92 percent / sodium hydride / dimethylformamide / Ambient temperature

6: 76 percent / 9-borabicyclo<3,3,1>nonane, aq. sodium hydroxide, hydrogen peroxide / ethanol

With sodium hydroxide; lithium aluminium tetrahydride; 9-borabicyclo[3.3.1]nonane dimer; dihydrogen peroxide; phosphorus tribromide; sodium hydride; potassium carbonate; In tetrahydrofuran; diethyl ether; ethanol; N,N-dimethyl-formamide; acetone;