Carbonic acid, 4-nitrophenyl 1-phenylethyl ester, (R)-

Base Information

• Chemical Name: Carbonic acid, 4-nitrophenyl 1-phenylethyl ester, (R)-
• CAS No.: 110884-69-0
• Molecular Formula: C15H13NO5
• Molecular Weight: 287.272
• Mol file: 110884-69-0.mol

Synonyms:carbonic acid 4-nitrophenyl ester (R)-1-phenylethyl ester;(+)-(R)-p-nitrophenyl 1-phenylethyl carbonate;Carbonic acid 4-nitro-phenyl ester (R)-1-phenyl-ethyl ester;4-nitrophenyl (R)-1-phenylethyl carbonate;

Chemical Property of Carbonic acid, 4-nitrophenyl 1-phenylethyl ester, (R)-

Chemical Property:

• PSA: 81.35000
• LogP: 4.39460

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Carbonic acid, 4-nitrophenyl 1-phenylethyl ester, (R)-

There total 2 articles about Carbonic acid, 4-nitrophenyl 1-phenylethyl ester, (R)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

(R)-1-phenylethanol (1517-69-7) + 4-Nitrophenyl chloroformate (7693-46-1) → Carbonic acid 4-nitrophenyl (R)-1-phenylethyl diester (110884-69-0)

Guidance literature:

With pyridine; In dichloromethane; Ambient temperature;

DOI:10.1021/jo00108a044

Reference yield:

→ Carbonic acid 4-nitrophenyl (R)-1-phenylethyl diester (110884-69-0)

Guidance literature:

Reference yield: 41.0%

Carbonic acid 4-nitrophenyl (R)-1-phenylethyl diester (110884-69-0) + 3-amino-5-phenyl-1,3-dihydrobenzo[e][1,4]diazepin-2-one (103343-47-1) → 1,3-Dihydro-5-phenyl-3(S)-<<(R)-α-methylbenzyloxycarbonyl>amino>-2H-1,4-benzodiazepin-2-one (161443-31-8) + 1,3-Dihydro-5-phenyl-3(R)-<<(R)-α-methylbenzyloxycarbonyl>amino>-2H-1,4-benzodiazepin-2-one

Guidance literature:

With triethylamine; In acetonitrile; Yields of byproduct given; Heating;

DOI:10.1021/jo00108a044

upstream raw materials:

(R)-1-phenylethanol

4-Nitrophenyl chloroformate

Downstream raw materials:

1,3-Dihydro-5-phenyl-3(S)-<<(R)-α-methylbenzyloxycarbonyl>amino>-2H-1,4-benzodiazepin-2-one

1,3-Dihydro-1-methyl-5-phenyl-3(S)-<<(R)-α-methylbenzyloxycarbonyl>amino>-2H-1,4-benzodiazepin-2-one

((2S,3S)-7-carbamoyl-1,1-diethyl-3-methoxy-1,2,3,4-tetrahydro-naphthalen-2-yl)-carbamic acid (R)-1-phenyl-ethyl ester

((2R,3R)-7-Carbamoyl-1,1-diethyl-3-methoxy-1,2,3,4-tetrahydro-naphthalen-2-yl)-carbamic acid (R)-1-phenyl-ethyl ester

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