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4-Nitrophenyl chloroformate Manufacturer/High quality/Best price/In stock
Cas No: 7693-46-1
USD $ 3.0-3.0 / Kilogram 1 Kilogram 1-100 Metric Ton/Month Dayang Chem (Hangzhou) Co.,Ltd. Contact Supplier
High quality 4-Nitrophenyl Chloroformate supplier in China
Cas No: 7693-46-1
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4 Nitrophenyl chloroformate 7693-46-1
Cas No: 7693-46-1
No Data 25 Kilogram 5000 Metric Ton/Month Hefei TNJ chemical industry co.,ltd Contact Supplier
4-Nitrophenyl ChloroforMate
Cas No: 7693-46-1
No Data 1 Kilogram 20 Metric Ton/Month Henan Allgreen Chemical Co.,Ltd Contact Supplier
Manufacturer high quality 4-Nitrophenyl chloroformate CAS NO.: 7693-46-1
Cas No: 7693-46-1
USD $ 60.0-80.0 / Kilogram 1 Kilogram 5000 Metric Ton/Month Xi'an Julong Bio-Tech Co., Ltd. Contact Supplier
4-Nitrophenyl chloroformate
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No Data 10 Milligram Amadis Chemical Co., Ltd. Contact Supplier
4-Nitrophenyl chloroformate
Cas No: 7693-46-1
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4-Nitrophenyl chloroformate CAS: 7693-46-1
Cas No: 7693-46-1
USD $ 1.0-2.0 / Metric Ton 5 Metric Ton 2500 Metric Ton/Year Henan Sinotech Import&Export Corporation Contact Supplier
7693-46-1 4-Nitrophenyl chloridocarbonate
Cas No: 7693-46-1
USD $ 8900.0-8900.0 / Gram 1 Gram 200 Gram/Day Henan Tianfu Chemical Co., Ltd. Contact Supplier
Factory Supply 4-Nitrophenyl chloroformate
Cas No: 7693-46-1
USD $ 1.0-3.0 / Gram 1 Gram 5 Kilogram/Day Ality Chemical Corporation Contact Supplier

7693-46-1 Usage

Uses

4-Nitrophenyl Chloroformate is an ester of chloroformic acid used in the immobilization of enzymes and other biomolecules.

Chemical Properties

Cream solid
InChI:InChI=1/C7H4ClNO4/c8-7(10)13-6-3-1-5(2-4-6)9(11)12/h1-4H

7693-46-1 Well-known Company Product Price

Brand (Code)Product description CAS number Packaging Price Detail
Aldrich (160210)  4-Nitrophenylchloroformate  96% 7693-46-1 160210-100G 2,315.43CNY Detail
Aldrich (160210)  4-Nitrophenylchloroformate  96% 7693-46-1 160210-25G 809.64CNY Detail
Aldrich (160210)  4-Nitrophenylchloroformate  96% 7693-46-1 160210-5G 281.97CNY Detail
Alfa Aesar (A18742)  4-Nitrophenyl chloroformate, 97%    7693-46-1 100g 1364.0CNY Detail
Alfa Aesar (A18742)  4-Nitrophenyl chloroformate, 97%    7693-46-1 25g 452.0CNY Detail
Alfa Aesar (A18742)  4-Nitrophenyl chloroformate, 97%    7693-46-1 5g 157.0CNY Detail
TCI America (C1400)  4-Nitrophenyl Chloroformate  >98.0%(T) 7693-46-1 250g 2,490.00CNY Detail
TCI America (C1400)  4-Nitrophenyl Chloroformate  >98.0%(T) 7693-46-1 25g 490.00CNY Detail

7693-46-1SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 12, 2017

Revision Date: Aug 12, 2017

1.Identification

1.1 GHS Product identifier

Product name 4-Nitrophenyl chloroformate

1.2 Other means of identification

Product number -
Other names Nitrophenyl chloroforMate

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only.
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:7693-46-1 SDS

7693-46-1Synthetic route

4-nitro-phenol
100-02-7

4-nitro-phenol

bis(trichloromethyl) carbonate
32315-10-9

bis(trichloromethyl) carbonate

4-Nitrophenyl chloroformate
7693-46-1

4-Nitrophenyl chloroformate

Conditions
ConditionsYield
With N,N-diethylaniline In toluene at 0℃; for 1h;95%
With N-ethyl-N,N-diisopropylamine In 1,2-dichloro-ethane at 75℃; for 0.5h; Inert atmosphere;
With triethylamine In tetrahydrofuran at 0 - 20℃; for 6.25h; Inert atmosphere;
phosgene
75-44-5

phosgene

4-nitro-phenol
100-02-7

4-nitro-phenol

4-Nitrophenyl chloroformate
7693-46-1

4-Nitrophenyl chloroformate

Conditions
ConditionsYield
With potassium carbonate In dichloromethane at 25℃; Green chemistry;92%
With N,N-dimethyl-aniline; triethylamine
4-nitro-phenol
100-02-7

4-nitro-phenol

trichloromethyl chloroformate
503-38-8

trichloromethyl chloroformate

4-Nitrophenyl chloroformate
7693-46-1

4-Nitrophenyl chloroformate

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine In dichloromethane 1.) 0 deg C, 0.5 h, 2.) reflux, 2 h;90%
With N-ethyl-N,N-diisopropylamine In dichloromethane Heating;36%
phosgene
75-44-5

phosgene

4-nitrophenol sodium salt
824-78-2

4-nitrophenol sodium salt

4-Nitrophenyl chloroformate
7693-46-1

4-Nitrophenyl chloroformate

phosgene
75-44-5

phosgene

sodium salt of p-nitro-phenol

sodium salt of p-nitro-phenol

4-Nitrophenyl chloroformate
7693-46-1

4-Nitrophenyl chloroformate

Conditions
ConditionsYield
With benzene
3-amino-1-methyl-5-phenyl-1,3-dihydro-2H-1,4-benzodiazepin-2-one
103421-61-0

3-amino-1-methyl-5-phenyl-1,3-dihydro-2H-1,4-benzodiazepin-2-one

m-phenylenediamine
108-45-2

m-phenylenediamine

A

N-{1,3-Dihydro-1-methyl-2-oxo-5-phenyl-1H-1,4-benzodiazepin-3-yl}-N'-{[3-(amino)phenyl]urea}

N-{1,3-Dihydro-1-methyl-2-oxo-5-phenyl-1H-1,4-benzodiazepin-3-yl}-N'-{[3-(amino)phenyl]urea}

B

4-Nitrophenyl chloroformate
7693-46-1

4-Nitrophenyl chloroformate

Conditions
ConditionsYield
With triethylamine In N,N-dimethyl-formamide
4-nitro-phenol
100-02-7

4-nitro-phenol

4-Nitrophenyl chloroformate
7693-46-1

4-Nitrophenyl chloroformate

Conditions
ConditionsYield
Stage #1: 4-nitro-phenol With bis(trichloromethyl) carbonate In dichloromethane at 0℃;
Stage #2: With N-ethyl-N,N-diisopropylamine In dichloromethane at 0 - 20℃; Heating / reflux;
dexamethasone
50-02-2

dexamethasone

4-Nitrophenyl chloroformate
7693-46-1

4-Nitrophenyl chloroformate

dexamethasone 21-(p-nitrophenyl carbonate)
79360-11-5

dexamethasone 21-(p-nitrophenyl carbonate)

Conditions
ConditionsYield
With pyridine In chloroform Ambient temperature;100%
With pyridine In dichloromethane at 20℃; for 0.4h; Sealed tube;72%
With 4-methyl-morpholine In tetrahydrofuran at 20℃; for 24h;55%
With 4-methyl-morpholine In tetrahydrofuran at 20℃; for 4h;
With pyridine at 20℃; for 2h; Concentration;
4-Nitrophenyl chloroformate
7693-46-1

4-Nitrophenyl chloroformate

5-O-(tert-butyldimethylsilyl)avermectin B1a
81924-41-6

5-O-(tert-butyldimethylsilyl)avermectin B1a

5-O-(tert-butyldimethylsilyl)-4''-O-<<(4-nitrophenyl)oxy>carbonyl>avermectin B1a
81924-49-4

5-O-(tert-butyldimethylsilyl)-4''-O-<<(4-nitrophenyl)oxy>carbonyl>avermectin B1a

Conditions
ConditionsYield
With dmap; N-ethyl-N,N-diisopropylamine In dichloromethane at 0℃; for 1h;100%
4-Nitrophenyl chloroformate
7693-46-1

4-Nitrophenyl chloroformate

3',5'-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)uridine
69304-38-7

3',5'-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)uridine

2′-O-(4-nitrophenoxycarbonyl)-3′,5′-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)uridine
202533-73-1

2′-O-(4-nitrophenoxycarbonyl)-3′,5′-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)uridine

Conditions
ConditionsYield
With pyridine; dmap at 20℃; for 16h;100%
In pyridine; toluene for 1h; Ambient temperature;96%
With pyridine In toluene at 20℃; for 5h; Inert atmosphere;81%
morpholine
110-91-8

morpholine

4-Nitrophenyl chloroformate
7693-46-1

4-Nitrophenyl chloroformate

morpholine-4-carboxylic acid 4-nitrophenyl ester
17376-42-0

morpholine-4-carboxylic acid 4-nitrophenyl ester

Conditions
ConditionsYield
With triethylamine In dichloromethane at 20℃; for 3.5h;100%
With triethylamine In dichloromethane at 20℃; for 3.5h;100%
With triethylamine In dichloromethane at 0 - 20℃; for 3h; Acylation;58%
tert-butyl (1S)-1-(chloromethyl)-5-hydroxy-1,2-dihydro-3H-benzo[e]indole-3-carboxylate
122745-41-9, 130008-89-8, 130007-86-2

tert-butyl (1S)-1-(chloromethyl)-5-hydroxy-1,2-dihydro-3H-benzo[e]indole-3-carboxylate

4-Nitrophenyl chloroformate
7693-46-1

4-Nitrophenyl chloroformate

(S)-tert-butyl 1-(chloromethyl)-5-((4-nitrophenoxy)carbonyloxy)-1H-benzo[e]indole-3(2H)-carboxylate

(S)-tert-butyl 1-(chloromethyl)-5-((4-nitrophenoxy)carbonyloxy)-1H-benzo[e]indole-3(2H)-carboxylate

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine In tetrahydrofuran at 0 - 20℃;100%
With triethylamine In dichloromethane at 25℃; for 2h; Substitution;
With N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 5h;
4-Nitrophenyl chloroformate
7693-46-1

4-Nitrophenyl chloroformate

(2-Phenyl-2-trimethylsilyl)ethanol
122760-31-0

(2-Phenyl-2-trimethylsilyl)ethanol

(2-Phenyl-2-trimethylsilyl)ethyl 4-nitrophenyl carbonate
327026-58-4

(2-Phenyl-2-trimethylsilyl)ethyl 4-nitrophenyl carbonate

Conditions
ConditionsYield
With pyridine In dichloromethane at 20℃; for 4h;100%
4-azidobenzyl alcohol
31499-54-4

4-azidobenzyl alcohol

4-Nitrophenyl chloroformate
7693-46-1

4-Nitrophenyl chloroformate

2'-(4-azidobenzyloxycarbonyl)paclitaxel

2'-(4-azidobenzyloxycarbonyl)paclitaxel

Conditions
ConditionsYield
Stage #1: 4-azidobenzyl alcohol; 4-Nitrophenyl chloroformate With pyridine; dmap In dichloromethane for 0.666667h;
Stage #2: taxol With dmap In dichloromethane for 70h;
100%
4-Nitrophenyl chloroformate
7693-46-1

4-Nitrophenyl chloroformate

Nα-(9-fluorenylmethoxycarbonyl)-D-serine-tert-butyl ether
71989-33-8, 128107-47-1

Nα-(9-fluorenylmethoxycarbonyl)-D-serine-tert-butyl ether

3-tert-butoxy-2-(9H-fluoren-9-ylmethoxycarbonylamino)-propionic acid 4-nitro-phenyl ester
439905-03-0

3-tert-butoxy-2-(9H-fluoren-9-ylmethoxycarbonylamino)-propionic acid 4-nitro-phenyl ester

Conditions
ConditionsYield
Stage #1: 4-Nitrophenyl chloroformate; Nα-(9-fluorenylmethoxycarbonyl)-D-serine-tert-butyl ether With TEA In dichloromethane at 0℃; for 0.25h;
Stage #2: With dmap at 0℃; for 0.5h;
100%
4-Nitrophenyl chloroformate
7693-46-1

4-Nitrophenyl chloroformate

benzylamine
100-46-9

benzylamine

(6-hydroxymethyl-naphthalen-2-yl)-carbamic acid allyl ester
393521-87-4

(6-hydroxymethyl-naphthalen-2-yl)-carbamic acid allyl ester

(6-benzylcarbamoyloxymethyl-naphthalen-2-yl)-carbamic acid allyl ester
393521-89-6

(6-benzylcarbamoyloxymethyl-naphthalen-2-yl)-carbamic acid allyl ester

Conditions
ConditionsYield
Stage #1: 4-Nitrophenyl chloroformate; (6-hydroxymethyl-naphthalen-2-yl)-carbamic acid allyl ester In tetrahydrofuran; pyridine at 20℃; for 4h;
Stage #2: benzylamine In tetrahydrofuran; pyridine at 20℃; for 19h; Further stages.;
100%
4-Nitrophenyl chloroformate
7693-46-1

4-Nitrophenyl chloroformate

benzylamine
100-46-9

benzylamine

(4'-hydroxymethyl-biphenyl-4-yl)-carbamic acid allyl ester
393522-89-9

(4'-hydroxymethyl-biphenyl-4-yl)-carbamic acid allyl ester

(4'-benzylcarbamoyloxymethyl-biphenyl-4-yl)-carbamic acid allyl ester
393522-92-4

(4'-benzylcarbamoyloxymethyl-biphenyl-4-yl)-carbamic acid allyl ester

Conditions
ConditionsYield
Stage #1: 4-Nitrophenyl chloroformate; (4'-hydroxymethyl-biphenyl-4-yl)-carbamic acid allyl ester With triethylamine In tetrahydrofuran at 20℃; for 19h;
Stage #2: benzylamine In tetrahydrofuran for 21h; Further stages.;
100%
4-Nitrophenyl chloroformate
7693-46-1

4-Nitrophenyl chloroformate

C49H57N7O12
393522-16-2

C49H57N7O12

Carbonic acid 4-[4-(4-{(S)-6-allyloxycarbonylamino-2-[(S)-2-((R)-2-allyloxycarbonylamino-propionylamino)-3-phenyl-propionylamino]-hexanoylamino}-benzyloxycarbonylamino)-benzyloxycarbonylamino]-benzyl ester 4-nitro-phenyl ester
393522-19-5

Carbonic acid 4-[4-(4-{(S)-6-allyloxycarbonylamino-2-[(S)-2-((R)-2-allyloxycarbonylamino-propionylamino)-3-phenyl-propionylamino]-hexanoylamino}-benzyloxycarbonylamino)-benzyloxycarbonylamino]-benzyl ester 4-nitro-phenyl ester

Conditions
ConditionsYield
In tetrahydrofuran; pyridine; dichloromethane at -40 - 6℃; for 48h;100%
1-hydroxy-pyrrolidine-2,5-dione
6066-82-6

1-hydroxy-pyrrolidine-2,5-dione

4-Nitrophenyl chloroformate
7693-46-1

4-Nitrophenyl chloroformate

N-(4-nitrophenoxycarbonyloxy)succinimide
371783-15-2

N-(4-nitrophenoxycarbonyloxy)succinimide

Conditions
ConditionsYield
With triethylamine In tetrahydrofuran at 0℃; for 0.5h;100%
4-(diisopropylsilanyl)-phenyl methanol
475160-70-4

4-(diisopropylsilanyl)-phenyl methanol

4-Nitrophenyl chloroformate
7693-46-1

4-Nitrophenyl chloroformate

carbonic acid 4-(diisopropyl-silanyl)-benzyl ester 4-nitrophenyl ester

carbonic acid 4-(diisopropyl-silanyl)-benzyl ester 4-nitrophenyl ester

Conditions
ConditionsYield
With 2,6-dimethylpyridine In dichloromethane for 0.75h;100%
4-methoxy-aniline
104-94-9

4-methoxy-aniline

4-Nitrophenyl chloroformate
7693-46-1

4-Nitrophenyl chloroformate

4-nitrophenyl (4-methoxyphenyl)carbamate
4058-71-3

4-nitrophenyl (4-methoxyphenyl)carbamate

Conditions
ConditionsYield
With pyridine In dichloromethane for 72h;100%
With pyridine In dichloromethane at 20℃;
With sodium hydrogencarbonate In tetrahydrofuran at 0 - 20℃; for 2h; Inert atmosphere;
With pyridine In tetrahydrofuran at 0℃; Inert atmosphere;
4-methyl-benzaldehyde
104-87-0

4-methyl-benzaldehyde

4-Nitrophenyl chloroformate
7693-46-1

4-Nitrophenyl chloroformate

O-(4-nitrophenyl)-N-(4-tolyl)carbamate
3848-42-8

O-(4-nitrophenyl)-N-(4-tolyl)carbamate

Conditions
ConditionsYield
With pyridine In dichloromethane at 20℃; for 0.5h;100%
4-Nitrophenyl chloroformate
7693-46-1

4-Nitrophenyl chloroformate

4-(2-keto-1-benzimidazolinyl)piperidine
20662-53-7

4-(2-keto-1-benzimidazolinyl)piperidine

C19H18N4O5
633312-78-4

C19H18N4O5

Conditions
ConditionsYield
With triethylamine In 1,2-dichloro-ethane100%
With triethylamine In 1,2-dichloro-ethane for 1h; Heating / reflux;100%
(8E,12E,14E)-7-acetoxy-6,21-dihydroxy-6,10,12,16,20-pentamethyl-3-(4-nitrophenoxycarboxy)-18,19-epoxytricosa-8,12,14-trien-11-olide

(8E,12E,14E)-7-acetoxy-6,21-dihydroxy-6,10,12,16,20-pentamethyl-3-(4-nitrophenoxycarboxy)-18,19-epoxytricosa-8,12,14-trien-11-olide

4-Nitrophenyl chloroformate
7693-46-1

4-Nitrophenyl chloroformate

(8E,12E,14E)-7-acetoxy-3-carbamoyloxy-6,21-dihydroxy-6,10,12,16,20-pentamethyl-18,19-epoxytricosa-8,12,14-trien-11-olide

(8E,12E,14E)-7-acetoxy-3-carbamoyloxy-6,21-dihydroxy-6,10,12,16,20-pentamethyl-18,19-epoxytricosa-8,12,14-trien-11-olide

Conditions
ConditionsYield
With ammonia In tetrahydrofuran; water for 21.5h;100%
L-tert-leucine methyl ester hydrochloride
63038-27-7

L-tert-leucine methyl ester hydrochloride

4-Nitrophenyl chloroformate
7693-46-1

4-Nitrophenyl chloroformate

methyl (2S)-3,3-dimethyl-2-{[(4-nitrophenoxy)carbonyl]amino}butanoate
854755-78-5

methyl (2S)-3,3-dimethyl-2-{[(4-nitrophenoxy)carbonyl]amino}butanoate

Conditions
ConditionsYield
With 4-methyl-morpholine In dichloromethane at 25℃; for 64h;100%
methyl 2(S)-ethoxy-3-[6-(3-methylaminophenyl)pyrid-3-yl]propanoate
817618-70-5

methyl 2(S)-ethoxy-3-[6-(3-methylaminophenyl)pyrid-3-yl]propanoate

4-Nitrophenyl chloroformate
7693-46-1

4-Nitrophenyl chloroformate

methyl 2(S)-ethoxy-3-(6-{3-[methyl(4-nitrophenoxycarbonyl)amino]phenyl}pyrid-3-yl)propanoate
817618-71-6

methyl 2(S)-ethoxy-3-(6-{3-[methyl(4-nitrophenoxycarbonyl)amino]phenyl}pyrid-3-yl)propanoate

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 2h;100%
methyl 2(S)-ethoxy-3-[4-(6-methylaminopyrid-2-yl)phenyl]propanoate
817618-76-1

methyl 2(S)-ethoxy-3-[4-(6-methylaminopyrid-2-yl)phenyl]propanoate

4-Nitrophenyl chloroformate
7693-46-1

4-Nitrophenyl chloroformate

methyl 2(S)-ethoxy-3-(4-{6-[methyl(4-nitrophenoxycarbonyl)amino]pyrid-2-yl}phenyl)propanoate
817618-75-0

methyl 2(S)-ethoxy-3-(4-{6-[methyl(4-nitrophenoxycarbonyl)amino]pyrid-2-yl}phenyl)propanoate

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 1.5h;100%
(R)-methyl 2-hydroxy-3-(2-(methoxymethyl)-7-methyl-2H-indazol-5-yl)propanoate
855778-06-2

(R)-methyl 2-hydroxy-3-(2-(methoxymethyl)-7-methyl-2H-indazol-5-yl)propanoate

4-Nitrophenyl chloroformate
7693-46-1

4-Nitrophenyl chloroformate

(R)-methyl 3-(2-(methoxymethyl)-7-methyl-2H-indazol-5-yl)-2-((4-nitrophenoxy)carbonyloxy)propanoate
855778-07-3

(R)-methyl 3-(2-(methoxymethyl)-7-methyl-2H-indazol-5-yl)-2-((4-nitrophenoxy)carbonyloxy)propanoate

Conditions
ConditionsYield
With dmap; N-ethyl-N,N-diisopropylamine In dichloromethane at 0℃;100%
With dmap; N-ethyl-N,N-diisopropylamine In dichloromethane at 0℃;100%
methyl 3-(2-((2-(trimethylsilyl)ethoxy)methyl)-7-methyl-2H-indazol-5-yl)-2-hydroxypropanoate
855778-80-2

methyl 3-(2-((2-(trimethylsilyl)ethoxy)methyl)-7-methyl-2H-indazol-5-yl)-2-hydroxypropanoate

4-Nitrophenyl chloroformate
7693-46-1

4-Nitrophenyl chloroformate

1-(methoxycarbonyl)-2-(2-((2-(trimethylsilyl)ethoxy)methyl)-7-methyl-2H-indazol-5-yl)ethyl 4-nitrophenyl carbonate
855778-81-3

1-(methoxycarbonyl)-2-(2-((2-(trimethylsilyl)ethoxy)methyl)-7-methyl-2H-indazol-5-yl)ethyl 4-nitrophenyl carbonate

Conditions
ConditionsYield
With pyridine at 20℃;100%
With pyridine at 20℃;100%
(8E,12E,14E)-7-hydroxy-6,10,12,16,20-pentamethyl-3,16,21-tris(triethylsiloxy)-18,19-epoxytricosa-8,12,14-trien-11-olide

(8E,12E,14E)-7-hydroxy-6,10,12,16,20-pentamethyl-3,16,21-tris(triethylsiloxy)-18,19-epoxytricosa-8,12,14-trien-11-olide

4-Nitrophenyl chloroformate
7693-46-1

4-Nitrophenyl chloroformate

(8E,12E,14E)-6,10,12,16,20-pentamethyl-7-((4-nitrophenoxy)carboxy)-3,16,21-tris(triethylsiloxy)-18,19-epoxytricosa-8,12,14-trien-11-olide

(8E,12E,14E)-6,10,12,16,20-pentamethyl-7-((4-nitrophenoxy)carboxy)-3,16,21-tris(triethylsiloxy)-18,19-epoxytricosa-8,12,14-trien-11-olide

Conditions
ConditionsYield
With dmap; triethylamine In dichloromethane at 5℃; for 1h;100%
(R)-2-hydroxy-3-(7-methyl-2-((2-(trimethylsilyl)ethoxy)methyl)-2H-indazol-5-yl)-1-(4-(piperidin-1-yl)piperidin-1-yl)propan-1-one
865626-75-1

(R)-2-hydroxy-3-(7-methyl-2-((2-(trimethylsilyl)ethoxy)methyl)-2H-indazol-5-yl)-1-(4-(piperidin-1-yl)piperidin-1-yl)propan-1-one

4-Nitrophenyl chloroformate
7693-46-1

4-Nitrophenyl chloroformate

(R)-3-(7-methyl-2-((2-(trimethylsilyl)ethoxy)methyl)-2H-indazol-5-yl)-1-oxo-1-(4-(piperidin-1-yl)piperidin-1-yl)propan-2-yl 4-nitrophenyl carbonate
865626-76-2

(R)-3-(7-methyl-2-((2-(trimethylsilyl)ethoxy)methyl)-2H-indazol-5-yl)-1-oxo-1-(4-(piperidin-1-yl)piperidin-1-yl)propan-2-yl 4-nitrophenyl carbonate

Conditions
ConditionsYield
With dmap; N-ethyl-N,N-diisopropylamine In dichloromethane at 0 - 20℃;100%
With dmap; N-ethyl-N,N-diisopropylamine In dichloromethane
tert-butyl 4-{[4-(aminomethyl)piperidin-1-yl]methyl}tetrahydro-2H-pyran-4-carboxylate
871021-84-0

tert-butyl 4-{[4-(aminomethyl)piperidin-1-yl]methyl}tetrahydro-2H-pyran-4-carboxylate

4-Nitrophenyl chloroformate
7693-46-1

4-Nitrophenyl chloroformate

tert-butyl 4-{[4-({[(3-isopropyl-2-oxo-2,3-dihydro-1H-benzimidazol-1-yl)carbonyl]amino}methyl)piperidin-1-yl]methyl}tetrahydro-2H-pyran-4-carboxylate
871021-85-1

tert-butyl 4-{[4-({[(3-isopropyl-2-oxo-2,3-dihydro-1H-benzimidazol-1-yl)carbonyl]amino}methyl)piperidin-1-yl]methyl}tetrahydro-2H-pyran-4-carboxylate

Conditions
ConditionsYield
Stage #1: 4-Nitrophenyl chloroformate; 1,3-dihydro-1-(1-methylethyl)-2H-benzimidazol-2-one With triethylamine In dichloromethane at 20℃; for 4h;
Stage #2: tert-butyl 4-{[4-(aminomethyl)piperidin-1-yl]methyl}tetrahydro-2H-pyran-4-carboxylate In dichloromethane at 20℃; for 24h;
100%
4-methyl-3-(1-{[4-(2,4,5-trifluorophenoxy)phenyl]methyl}(4-piperidyl))phenylamine
882745-59-7

4-methyl-3-(1-{[4-(2,4,5-trifluorophenoxy)phenyl]methyl}(4-piperidyl))phenylamine

4-Nitrophenyl chloroformate
7693-46-1

4-Nitrophenyl chloroformate

N-[4-methyl-3-(1-{[4-(2,4,5-trifluorophenoxy)phenyl]methyl}(4-piperidyl))phenyl](4-nitrophenoxy)carboxamide
882746-18-1

N-[4-methyl-3-(1-{[4-(2,4,5-trifluorophenoxy)phenyl]methyl}(4-piperidyl))phenyl](4-nitrophenoxy)carboxamide

Conditions
ConditionsYield
With pyridine In dichloromethane for 5h; Heating / reflux;100%
With pyridine In dichloromethane for 5h; Heating / reflux;100%
C17H16FN3OS*ClH

C17H16FN3OS*ClH

4-Nitrophenyl chloroformate
7693-46-1

4-Nitrophenyl chloroformate

C24H19FN4O5S

C24H19FN4O5S

Conditions
ConditionsYield
With pyridine In dichloromethane at 20℃; for 1h;100%
N-(2-aminoethyl)-2,3-dichloro-N-methylbenzenesulphonamide trifluoroacetate
1114225-30-7

N-(2-aminoethyl)-2,3-dichloro-N-methylbenzenesulphonamide trifluoroacetate

4-Nitrophenyl chloroformate
7693-46-1

4-Nitrophenyl chloroformate

4-nitrophenyl {2-[(2,3-dichlorobenzenesulphonyl)methylamino]ethyl}carbamate
886236-65-3

4-nitrophenyl {2-[(2,3-dichlorobenzenesulphonyl)methylamino]ethyl}carbamate

Conditions
ConditionsYield
With triethylamine In tetrahydrofuran at 0 - 20℃; for 1h;100%
(3R*,4R*)-N-[3,5-bis(trifluoromethyl)benzyl]-N-methyl-3-phenylpiperidine-4-carboxamide hydrochloride

(3R*,4R*)-N-[3,5-bis(trifluoromethyl)benzyl]-N-methyl-3-phenylpiperidine-4-carboxamide hydrochloride

4-Nitrophenyl chloroformate
7693-46-1

4-Nitrophenyl chloroformate

C29H25F6N3O5*ClH

C29H25F6N3O5*ClH

Conditions
ConditionsYield
Stage #1: (3R*,4R*)-N-[3,5-bis(trifluoromethyl)benzyl]-N-methyl-3-phenylpiperidine-4-carboxamide hydrochloride; 4-Nitrophenyl chloroformate With triethylamine In dichloromethane at 20℃; for 1h;
Stage #2: With ammonium chloride In dichloromethane; water; ethyl acetate
100%
3-{6-[2-(2,4-dichloro-phenyl)-ethylamino]-2-methoxy-pyrimidin-4-yl}-phenol
885066-89-7

3-{6-[2-(2,4-dichloro-phenyl)-ethylamino]-2-methoxy-pyrimidin-4-yl}-phenol

4-Nitrophenyl chloroformate
7693-46-1

4-Nitrophenyl chloroformate

carbonic acid 3-{6-[2-(2,4-dichloro-phenyl)-ethylamino]-2-methoxy-pyrimidin-4-yl}-phenyl ester 4-nitro-phenyl ester
885068-19-9

carbonic acid 3-{6-[2-(2,4-dichloro-phenyl)-ethylamino]-2-methoxy-pyrimidin-4-yl}-phenyl ester 4-nitro-phenyl ester

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 2h;100%
With N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 2h;100%

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